2,4,5-三甲基苯甲醛合成路线 (共 57 条)
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; P=760 Torr; 48 h; Yields of byproduct given;
参考文献
Tanaka, Mutsuo; Iyoda, Jun; Souma, Yoshie
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2677 - 2680
反应条件
TNM in various solvent(s) T=20°C; 0.5 h; Irradiation; Further byproducts given;
参考文献
Acta Chemica Scandinavica, , vol. 50, # 11 p. 991 - 1008
反应条件
nitrogen(IV) oxide in dichloromethane T=20°C; 0.5 h; in the dark; Further byproducts given. Title compound not separated from byproducts;
参考文献
Acta Chemica Scandinavica, , vol. 50, # 11 p. 991 - 1008
反应条件
[NO][PF6]; oxygen in dichloromethane T=3°C; 4.5 h;
参考文献
Journal of Organic Chemistry, , vol. 54, # 7 p. 1692 - 1702
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; P=760 Torr; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 57, # 9 p. 2677 - 2680
反应条件
formaldehyd; ethanol
参考文献
Journal of the American Chemical Society, , vol. 75, p. 2654,2656
反应条件
dinitrogen tetraoxide in dichloromethane T=25°C; 1.5 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 12 p. 3314 - 3325
反应条件
sodium cyanide; aluminium trichloride T=95 - 100°C; Einleiten von HCl und Eintragen des Reaktionsgemisches in Eis und wss. HCl;
参考文献
Journal of Organic Chemistry, , vol. 8, p. 147,148
反应条件
sodium cyanide; aluminium trichloride T=95 - 100°C; Einleiten von HCl und Eintragen des Reaktionsgemisches in Eis und wss. HCl;
参考文献
Journal of Organic Chemistry, , vol. 8, p. 147,148
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 39, # 1 p. 195 - 198