2,4,5-三甲基苯甲醛合成路线 (共 57 条)
反应条件
nitric acid; acetic anhydride 1 h; Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 111, # 6 p. 2263 - 2276
反应条件
sulfur T=220 - 230°C;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 34, p. 1571 - 1583
反应条件
toluene-4-sulfonic acid in xylene
参考文献
Bulletin of the Chemical Society of Japan, , vol. 34, p. 1571 - 1583
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 24 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 12 p. 3846 - 3850
反应条件
nitrogen(IV) oxide in dichloromethane T=20°C; 4 h; Irradiationwithout irradiation; Product distribution;
参考文献
Acta Chemica Scandinavica, , vol. 50, # 11 p. 991 - 1008
参考文献
Tetrahedron Letters, , vol. 28, # 30 p. 3479 - 3482
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 1 h; Yields of byproduct given;
参考文献
Tanaka, Mutsuo; Fujiwara, Masahiro; Ando, Hisanori
Journal of Organic Chemistry, 1995 , vol. 60, # 12 p. 3846 - 3850
反应条件
1: 140 - 150 °C 2: sulfur / 220 - 230 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 34, p. 1571 - 1583
反应条件
tetrahydrofuran; lithium aluminium tetrahydride
参考文献
Chemische Berichte, , vol. 88, p. 301,307
反应条件
sulfuric acid; acetic acid Heating;
参考文献
Canadian Journal of Chemistry, , vol. 54, p. 1795 - 1806