反应条件
1: 1.) PhLi / 1.) ether, rt, 2 h, 2.) THF, -78 deg C, 1 h
2: 100 percent / Ag2O, K2CO3 / acetonitrile / Ambient temperature
3: 1.) LiAlH4, 2.a) aq. NH4Cl, b) trifluoroacetic anhydride, pyridine / 1.) THF, -78 deg C, 0.5 h, 2.b) ether, 0 deg C
4: 2.) aq. ceric ammonium nitrate / 1.) o-xylene, 140 deg C, 3.5 h, 2.) CH3CN, rt
View Scheme
参考文献
Liebeskind, Lanny S.; Granberg, Kenneth L.; Zhang, Jing
Journal of Organic Chemistry, 1992 , vol. 57, # 16 p. 4345 - 4352
