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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴苯甲醚
合成路线
（共 581 条）
578-57-4
2-溴苯甲醚
+
563-47-3
3-氯-2-甲基丙烯
→
反应条件
91969-32-3
1-甲氧基-2-(2-甲基丙-2-烯基)苯
反应条件
(i) Mg, (ii) /BRN= 878160/; Multistep reaction;
参考文献
Ruechardt,C.; Eichler,S.
Chemische Berichte, 1962 , vol. 95, p. 1921 - 1942
848170-27-4
+
578-57-4
2-溴苯甲醚
→
反应条件
920508-13-0
反应条件
1: 2-methoxybromobenzene With n-butyllithium in diethyl ether T=-78°C; 2: indan-1-carboxylic acid methoxy-methyl-amide in diethyl ether
参考文献
Daum, Sebastian; Erdmann, Frank; Fischer, Gunter; De Lacroix, Boris Feaux; Hessamian-Alinejad, Anahita; Houben, Sabine; Frank, Walter; Braun, Manfred
Angewandte Chemie - International Edition, 2006 , vol. 45, # 44 p. 7454 - 7458
→
反应条件
920508-13-0
反应条件
1: 2-methoxybromobenzene With n-butyllithium in diethyl ether T=-78°C; 2: lithium; indan-1-carboxylate in diethyl ether
参考文献
Daum, Sebastian; Erdmann, Frank; Fischer, Gunter; De Lacroix, Boris Feaux; Hessamian-Alinejad, Anahita; Houben, Sabine; Frank, Walter; Braun, Manfred
Angewandte Chemie - International Edition, 2006 , vol. 45, # 44 p. 7454 - 7458
→
反应条件
92495-53-9
反应条件
palladium diacetate in water; N,N-dimethyl-formamide T=20°C; 5 h;
参考文献
WAKO PURE CHEMICAL INDUSTRIES, LTD.
Patent: US2010/87646 A1, 2010 ;
Location in patent: Page/Page column 16 ;
578-57-4
2-溴苯甲醚
+
725735-32-0
→
反应条件
92495-53-9
反应条件
1: triallyl(4-methylphenyl)silane With tetrabutyl ammonium fluoride in water; dimethyl sulfoxide T=20°C; 1 h; 2: 2-methoxybromobenzene With tri-cyclo-hexyl-phosphine; palladium dichloride in water; dimethyl sulfoxide T=80°C; 6 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
578-57-4
2-溴苯甲醚
+
5720-05-8
4-甲基苯硼酸
→
反应条件
92495-53-9
反应条件
potassium carbonate; palladium dichloride in ethanol; water T=20°C; Suzuki-Miyaura reaction; 0.25 h;
参考文献
Liu, Chun; Ni, Qijian; Hu, Pingping; Qiu, Jieshan
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 4 p. 1054 - 1060
578-57-4
2-溴苯甲醚
+
31614-66-1
→
反应条件
92495-53-9
反应条件
cesium fluoride in 1,4-dioxane T=100 - 110°C; Stille Cross Coupling; 20 h;
参考文献
Nasrollahzadeh, Mahmoud; Maham, Mehdi; Ehsani, Ali; Khalaj, Mehdi
RSC Advances, 2014 , vol. 4, # 38 p. 19731 - 19736
578-57-4
2-溴苯甲醚
+
106-38-7
对溴甲苯
→
反应条件
92495-53-9
反应条件
1: para-bromotoluene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran; hexane T=-78 - 20°C; 1 h; Inert atmosphere; 3: 2-methoxybromobenzene With XPhos G3; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; hexane T=75°C; Negishi Coupling; 12 h; Inert atmosphere;
参考文献
Yang, Yang; Oldenhuis, Nathan J.; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 2 p. 615 - 619
Angew. Chem., 2013 , vol. 125, # 2 p. 643 - 647,5
578-57-4
2-溴苯甲醚
+
195062-57-8
对甲基苯硼酸频哪醇酯
→
反应条件
92495-53-9
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium hydroxide in neat (no solvent) T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk techniqueInert atmosphere; Reagent/catalyst;
参考文献
Asachenko, Andrey F.; Sorochkina, Kristina R.; Dzhevakov, Pavel B.; Topchiy, Maxim A.; Nechaev, Mikhail S.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3553 - 3557
578-57-4
2-溴苯甲醚
+
18412-57-2
三乙氧基对苯甲基硅烷
→
反应条件
92495-53-9
反应条件
sodium hydroxide in water T=90°C; Hiyama coupling; 6 h;
参考文献
Sreedhar; Kumar, A. Suresh; Yada, Divya
Synlett, 2011 , # 8 art. no. D31410ST, p. 1081 - 1084
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