1: With hydrogenchloride in water T=0°C; 1.5 h; 2: With hydrogenchloride; sodium nitrite in water Cooling with ice; 3: With hydrogenchloride; tin(ll) chloride in water T=8°C; Cooling with ice;
参考文献
Fathalipour, Soghra; Shahrokhnia, Nazila; Afghan, Arash; Baradarani, Mehdi M.
Asian Journal of Chemistry, 2010 , vol. 22, # 8 p. 5808 - 5814
in ethanol; chloroform air atmosphere; addn. of stoich. amt. of metal salt (in EtOH) to soln. of ligand (in CHCl3), stirring (room temp., 2 h, pptn.); filtration, washing (CHCl3), drying (over CaCl2/P4O10); elem. anal.;
参考文献
Donia; El-Boraey
Journal of Thermal Analysis and Calorimetry, 1997 , vol. 48, # 6 p. 1325 - 1336
in water aq. solns. K2PdCl4 and ligand in excess hot water in 1:1 mole ratio mixed together and heated on water bath for 8-12 h; solid collected under suction, washed with hot water and dried under vac.; elem. anal.;
参考文献
Umapathy, P.; Harnesswala, Rashida A.; Dorai, C. S.
Polyhedron, 1985 , vol. 4, p. 1595 - 1602
