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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
7-甲基鸟嘌呤
合成路线
（共 22 条）
→
反应条件
578-76-7
7-甲基鸟嘌呤
反应条件
1: in isobutyramide T=20°C; 6 h; 2: With hydrogenchloride in water T=100°C; 1 h; 3: With ammonia in water T=0°C; pH=8;
参考文献
HERCULES TECHNOLOGY MANAGEMENT CO V, INC.; BLAGG, Julian
Patent: WO2011/35009 A1, 2011 ;
Location in patent: Page/Page column 48 ;
20244-86-4
7-甲基鸟苷
+
623925-45-1
→
反应条件
578-76-7
7-甲基鸟嘌呤
反应条件
sodium hydroxide; dipotassium hydrogenphosphate; purine nucleoside phosphorylase in water T=30°C; pH=7.4; 48 h; Enzymatic reaction;
参考文献
Shallop, Anthony J; Gaffney, Barbara L; Jones, Roger A
The Journal of organic chemistry, 2003 , vol. 68, # 22 p. 8657 - 8661
22164-16-5
+
66224-66-6
→
反应条件
578-76-7
7-甲基鸟嘌呤
+
58-61-7
腺苷
反应条件
potassium dihydrogenphosphate; purine nucleoside phosphorylase in water T=60°C; 22 h; pH 7.0;
参考文献
Voegel; Altorfer; Benner
Helvetica Chimica Acta, 1993 , vol. 76, # 5 p. 2061 - 2069
81100-62-1
+
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
2004-07-1
6-氯鸟嘌呤核苷
+
578-76-7
7-甲基鸟嘌呤
反应条件
recombinant purine nucleoside phosphorylase from Aeromonas hydrophila T=20°C; pH=7.5; aq. phosphate bufferEnzymatic reaction; regioselective reaction;
参考文献
Ubiali, Daniela; Serra, Carla D.; Serra, Immacolata; Morelli, Carlo F.; Terreni, Marco; Albertini, Alessandra M.; Manitto, Paolo; Speranzab, Giovanna
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 1 p. 96 - 104
81100-62-1
+
1198-47-6
2-氨基-6-巯嘌呤
→
反应条件
578-76-7
7-甲基鸟嘌呤
+
4914-73-2
反应条件
recombinant purine nucleoside phosphorylase from Aeromonas hydrophila T=20°C; pH=7.5; aq. phosphate bufferEnzymatic reaction; regioselective reaction;
参考文献
Ubiali, Daniela; Serra, Carla D.; Serra, Immacolata; Morelli, Carlo F.; Terreni, Marco; Albertini, Alessandra M.; Manitto, Paolo; Speranzab, Giovanna
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 1 p. 96 - 104
81100-62-1
+
1074-89-1
6-氯嘌呤
→
反应条件
578-76-7
7-甲基鸟嘌呤
+
5746-29-2
6-O-甲基肌苷
反应条件
recombinant purine nucleoside phosphorylase from Aeromonas hydrophila T=20°C; pH=7.5; aq. phosphate bufferEnzymatic reaction; regioselective reaction;
参考文献
Ubiali, Daniela; Serra, Carla D.; Serra, Immacolata; Morelli, Carlo F.; Terreni, Marco; Albertini, Alessandra M.; Manitto, Paolo; Speranzab, Giovanna
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 1 p. 96 - 104
81100-62-1
+
2004-03-7
6-甲基嘌呤
→
反应条件
578-76-7
7-甲基鸟嘌呤
+
14675-48-0
反应条件
recombinant purine nucleoside phosphorylase from Aeromonas hydrophila in glycerol T=20°C; pH=7.5; aq. phosphate bufferEnzymatic reaction; regioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 1 p. 96 - 104
66224-66-6
→
反应条件
578-76-7
7-甲基鸟嘌呤
+
958-09-8
2’-脱氧腺苷
反应条件
potassium dihydrogenphosphate; purine nucleoside phosphatase in water T=45°C; 16 h; enzymatic synthesis of various β-D-ribo (and desoxyribo) nucleoside analogs; effect of temperature: 25-60 deg C;
参考文献
Voegel; Altorfer; Benner
Helvetica Chimica Acta, 1993 , vol. 76, # 5 p. 2061 - 2069
66-27-3
甲磺酸甲酯
→
反应条件
964-21-6
2'-脱氧-6-O-甲基-鸟苷
+
578-76-7
7-甲基鸟嘌呤
+
60192-57-6
反应条件
in various solvent(s) T=20°C; Methylation; pH=7.8; 24 h;
参考文献
Chemical Research in Toxicology, , vol. 9, # 3 p. 563 - 567
→
反应条件
964-21-6
2'-脱氧-6-O-甲基-鸟苷
+
578-76-7
7-甲基鸟嘌呤
+
60192-57-6
反应条件
in various solvent(s) T=20°C; Methylation; pH=8.0; 24 h;
参考文献
Chemical Research in Toxicology, , vol. 9, # 3 p. 563 - 567
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