copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
T=20°C; 0.666667 h;
参考文献
Cox, Russell J.; Ritson, Dougal J.; Dane, Thomas A.; Berge, John; Charmant, Jonathan P. H.; Kantacha, Anob
Chemical Communications, 2005 , # 8 p. 1037 - 1039
1: With N-ethyl-N,N-diisopropylamine in dichloromethane
T=0 - 20°C; 4 h;
2: With sodium hydrogencarbonate in dichloromethane; water
3: With oxalyl dichloride; N,N-dimethyl-formamide
more than 3 stages;
参考文献
PHARMACIA and UPJOHN COMPANY LLC
Patent: WO2006/126082 A2, 2006 ;
Location in patent: Page/Page column 61 ;