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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5782-17-2
合成路线
（共 9 条）
696-62-8
4-碘苯甲醚
+
110598-51-1
→
反应条件
5782-17-2
反应条件
palladium diacetate; potassium carbonate; 2,2,2-trimethylacetic acid in N,N-dimethyl acetamide T=160°C; 12 h; Inert atmosphere;
参考文献
Guo, Lei; Zhang, Fengying; Hu, Weimin; Li, Lei; Jia, Yanxing
Chemical Communications, 2014 , vol. 50, # 25 p. 3299 - 3302
5661-50-7
+
2132-62-9
林可霉素 2,7-二乙酸酯
→
反应条件
5782-17-2
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate; acetic acid in dichloromethane T=20°C;
参考文献
Liu, Guixia; Shen, Yangyang; Zhou, Zhi; Lu, Xiyan
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6033 - 6037
Angew. Chem., 2013 , vol. 125, # 23 p. 6149 - 6153,5
118-93-4
2'-羟基苯乙酮
→
反应条件
5782-17-2
反应条件
1.1: tetrahydrofuran / 8 h / 0 °C / |Reflux 1.2: |Reflux 2.1: potassium carbonate; palladium diacetate; 2,2,2-trimethylacetic acid / N,N-dimethyl acetamide / 12 h / 160 °C / |Inert atmosphere View Scheme
参考文献
Guo, Lei; Zhang, Fengying; Hu, Weimin; Li, Lei; Jia, Yanxing
Chemical Communications, 2014 , vol. 50, # 25 p. 3299 - 3302
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
5782-17-2
反应条件
1.1: tetrahydrofuran / 8 h / 0 °C / |Reflux 1.2: |Reflux 2.1: potassium carbonate; palladium diacetate; 2,2,2-trimethylacetic acid / N,N-dimethyl acetamide / 12 h / 160 °C / |Inert atmosphere View Scheme
参考文献
Guo, Lei; Zhang, Fengying; Hu, Weimin; Li, Lei; Jia, Yanxing
Chemical Communications, 2014 , vol. 50, # 25 p. 3299 - 3302
4846-21-3
→
反应条件
5782-17-2
反应条件
1: sodium carbonate / ethyl acetate; water / 2 h / 0 °C 2: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate; acetic acid / dichloromethane / 20 °C View Scheme
参考文献
Liu, Guixia; Shen, Yangyang; Zhou, Zhi; Lu, Xiyan
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6033 - 6037
Angew. Chem., 2013 , vol. 125, # 23 p. 6149 - 6153,5
98-80-6
苯硼酸
→
反应条件
5782-17-2
反应条件
1: copper(l) chloride; pyridine / 1,2-dichloro-ethane / 48 h / 20 °C / |Molecular sieve 2: hydrazine hydrate / methanol; chloroform / 20 °C 3: sodium carbonate / ethyl acetate; water / 2 h / 0 °C 4: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate; acetic acid / dichloromethane / 20 °C View Scheme
参考文献
Liu, Guixia; Shen, Yangyang; Zhou, Zhi; Lu, Xiyan
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6033 - 6037
Angew. Chem., 2013 , vol. 125, # 23 p. 6149 - 6153,5
64908-64-1
→
反应条件
5782-17-2
反应条件
1: hydrazine hydrate / methanol; chloroform / 20 °C 2: sodium carbonate / ethyl acetate; water / 2 h / 0 °C 3: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate; acetic acid / dichloromethane / 20 °C View Scheme
参考文献
Liu, Guixia; Shen, Yangyang; Zhou, Zhi; Lu, Xiyan
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6033 - 6037
Angew. Chem., 2013 , vol. 125, # 23 p. 6149 - 6153,5
110598-51-1
→
反应条件
5782-17-2
反应条件
1: potassium carbonate; palladium diacetate; 2,2,2-trimethylacetic acid / N,N-dimethyl acetamide / 1 h / 160 °C / |Inert atmosphere 2: potassium carbonate; para-iodoanisole; palladium diacetate; 2,2,2-trimethylacetic acid / N,N-dimethyl acetamide / 8 h / 160 °C / |Inert atmosphere View Scheme
参考文献
Guo, Lei; Zhang, Fengying; Hu, Weimin; Li, Lei; Jia, Yanxing
Chemical Communications, 2014 , vol. 50, # 25 p. 3299 - 3302
119-52-8
烷异英
+
108-95-2
苯酚
→
反应条件
5782-17-2
反应条件
1,4-dioxane; hydrogenchloride
参考文献
Brown; Cummings
Journal of the Chemical Society, 1958 , p. 4302,4304
