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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5782-23-0
合成路线
（共 14 条）
120-72-9
吲哚
+
104-92-7
4-溴苯甲醚
→
反应条件
5782-23-0
反应条件
(benzyl)-tri-(butyl)-ammonium chloride; potassium carbonate; palladium diacetate in toluene T=110°C; 24 h;
参考文献
Bellina, Fabio; Benelli, Francesca; Rossi, Renzo
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5529 - 5535
104-92-7
4-溴苯甲醚
→
反应条件
5782-23-0
反应条件
1: 3-iodoindole-N-SO2-polystyrene With pinacol borane; triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in 1,4-dioxane T=80°C; 20 h; 2: 1-bromo-4-methoxy-benzene With potassium phosphate; Pd0(tris(tert-butyl)phosphine)2 in N,N-dimethyl-formamide T=80°C; Suzuki coupling reaction; 24 h; 3: With potassium tert-butylate in tetrahydrofuran T=20°C; 6 h;
参考文献
Kasahara, Takahiro; Kondo, Yoshinori
Heterocycles, 2006 , vol. 67, # 1 p. 95 - 100
696-62-8
4-碘苯甲醚
→
反应条件
5782-23-0
反应条件
1: 3-iodoindole-N-SO2-polystyrene With pinacol borane; triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in 1,4-dioxane T=80°C; 20 h; 2: para-iodoanisole With potassium phosphate; Pd0(tris(tert-butyl)phosphine)2 in N,N-dimethyl-formamide T=80°C; Suzuki coupling reaction; 24 h; 3: With potassium tert-butylate in tetrahydrofuran T=20°C; 6 h;
参考文献
Kasahara, Takahiro; Kondo, Yoshinori
Heterocycles, 2006 , vol. 67, # 1 p. 95 - 100
120-72-9
吲哚
+
104-92-7
4-溴苯甲醚
→
反应条件
5784-95-2
2-(4-甲氧基苯基)-1H-吲哚
+
5782-23-0
+
93597-01-4
1-(4-甲氧基苯基)吲哚
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium carbonate; palladium diacetate in toluene T=110°C; 48 h;
参考文献
Bellina, Fabio; Benelli, Francesca; Rossi, Renzo
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5529 - 5535
5703-26-4
4-甲氧基苯乙醛
+
100-63-0
苯肼
→
反应条件
5782-23-0
反应条件
zinc(II) chloride in ethanol T=100°C; 2 h; Inert atmosphereSchlenk technique;
参考文献
Nagase, Yuta; Shirai, Hiroyuki; Kaneko, Masayoshi; Shirakawa, Eiji; Tsuchimoto, Teruhisa
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 9 p. 1456 - 1459
120-72-9
吲哚
→
反应条件
5782-23-0
反应条件
in N,N-dimethyl-formamide T=100°C; 22 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Dellacqua, Monica; Fenner, Sabine; Vicente, Ruben; Sandmann, Rene
Organic Letters, 2011 , vol. 13, # 9 p. 2358 - 2360
100-65-2
N-苯基羟胺
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
5782-23-0
反应条件
Fe pythalocyanine in toluene RefluxInert atmosphere; regioselective reaction;
参考文献
Lamar, Angus A.; Nicholas, Kenneth M.
Tetrahedron, 2009 , vol. 65, # 19 p. 3829 - 3833
120-72-9
吲哚
+
104-92-7
4-溴苯甲醚
→
反应条件
5784-95-2
2-(4-甲氧基苯基)-1H-吲哚
+
5782-23-0
反应条件
lithium hydroxide hydrate; palladium diacetate; bis(1,1-diphenylphosphino)methane in water T=110°C; 18 h; regioselective reaction;
参考文献
Joucla, Lionel; Batail, Nelly; Djakovitch, Laurent
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 2929 - 2936
120-72-9
吲哚
→
反应条件
5782-23-0
+
81344-98-1
反应条件
in N,N-dimethyl-formamide T=100°C; 22 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Dellacqua, Monica; Fenner, Sabine; Vicente, Ruben; Sandmann, Rene
Organic Letters, 2011 , vol. 13, # 9 p. 2358 - 2360
696-62-8
4-碘苯甲醚
→
反应条件
5782-23-0
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in dimethyl sulfoxide T=40°C; 1.75 h;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Marinelli, Fabio; Moro, Leonardo; Pace, Paola
Synlett, 1997 , # 12 p. 1363 - 1366
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