2-乙氧基-5,5-二甲基-1,3-二恶烷合成路线 （共 13 条）
反应条件
toluene-4-sulfonic acid in n-heptane T=20 - 30°C; 0.5 h; other 2-ethoxy-1,3-dioxanes, other reagents; Product distribution;
参考文献
Zhurkina, I. P.; Nedogrei, E. P.; Musavirov, R. S.; Rakhmankulov, D. L.; Paushkin, Ya. M.
Doklady Chemistry, 1989 , vol. 304, # 1-6 p. 49 - 50
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 304, # 4 p. 883 - 885
反应条件
toluene-4-sulfonic acid in n-heptane T=60°C; 0.166667 h; Product distribution;
参考文献
Nedogrei, E. P.; Musavirov, R. C.; Zlomskii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 9 p. 2078 - 2081,1875 - 1877
反应条件
sulfuric acid in toluene T=40°C; 8 h; Yield given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 8 p. 1786 - 1792,1586 - 1592
反应条件
toluene-4-sulfonic acid in n-heptane T=20 - 30°C; 0.5 h; other 2-ethoxy-1,3-dioxanes, other reagents; Product distribution;
参考文献
Zhurkina, I. P.; Nedogrei, E. P.; Musavirov, R. S.; Rakhmankulov, D. L.; Paushkin, Ya. M.
Doklady Chemistry, 1989 , vol. 304, # 1-6 p. 49 - 50
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 304, # 4 p. 883 - 885
反应条件
zinc(II) chloride in diethyl ether temperature below 30 deg C;
参考文献
Imashev, U. B.; Kalashnikov, S. M.; Gordeeva, G. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 4 p. 369 - 373
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 4 p. 459 - 463
反应条件
sulfuric acid in toluene T=40°C; 8 h; Yield given;
参考文献
Musavirov, R. S.; Nedogrei, E. P.; Kantor, E. A.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1786 - 1792,1586 - 1592
反应条件
toluene-4-sulfonic acid in n-heptane T=20 - 30°C; 0.5 h; other 2-ethoxy-1,3-dioxanes, other reagents; Product distribution;
参考文献
Doklady Chemistry, , vol. 304, # 1-6 p. 49 - 50
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 304, # 4 p. 883 - 885
反应条件
hydrogenchloride in toluene T=40°C; 8 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 8 p. 1786 - 1792,1586 - 1592
反应条件
toluene-4-sulfonic acid
0.5 h;
参考文献
Sant, Milind P.; Smith, William B.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5479 - 5481
反应条件
toluene-4-sulfonic acid
T=100 - 110°C; 3 h;
参考文献
Lapuka, L. F.; Chalova, O. B.; Kantor, E. A.; Kiladze, T. K.; Rakhmankulov, D. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 9 p. 876 - 879
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , vol. 17, # 9 p. 1182 - 1185
