4,5-二溴-3[2H]-哒嗪酮合成路线 （共 8 条）
反应条件
sodium acetate; monohydrazine sulfate in ethanol; water T=60°C; 5 h; Reflux;
参考文献
Humphries, Paul S.; Oliver, Robert M.
Tetrahedron Letters, 2009 , vol. 50, # 22 p. 2682 - 2684
反应条件
in water T=15 - 17°C; 1.2 h;
参考文献
Kim, Jeum-Jong; Kweon, Deok-Heon; Cho, Su-Dong; Kim, Ho-Kyun; Jung, Eun-Young; Lee, Sang-Gyeong; Falck; Yoon, Yong-Jin
Tetrahedron, 2005 , vol. 61, # 24 p. 5889 - 5894
反应条件
trifluoroacetic acid in dichloromethane T=60°C; 12 h;
参考文献
Synlett, , # 8 p. 1113 - 1116
反应条件
sodium hydroxide; palladium on activated charcoal Hydrogenation;
参考文献
Grundmann
Chemische Berichte, 1948 , vol. 81, p. 1,10
反应条件
tetrabutylammomium bromide; potassium carbonate in acetonitrile T=20°C; Inert atmosphere;
参考文献
Verhelst, Tom; Verbeeck, Stefan; Ryabtsova, Oxana; Depraetere, Stefaan; Maes, Bert U. W.
Organic Letters, 2011 , vol. 13, # 2 p. 272 - 275
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Yamasaki, Tetsuo; Kawaminami, Eiji; Yamada, Tomomi; Okawara, Tadashi; Furukawa, Mitsuru
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 991 - 996
反应条件
potassium carbonate in N,N-dimethyl-formamide T=50 - 60°C; 2 h;
参考文献
Cho, Su-Dong; Choi, Woo-Yong; Yoon, Yong-Jin
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1579 - 1582
参考文献
Sotelo, Eddy; Coelho, Alberto; Ravina, Enrique
Tetrahedron Letters, 2003 , vol. 44, # 24 p. 4459 - 4462
