1-苯基-1,2-丙二酮合成路线 （共 223 条）
反应条件
1: TiCl4 / benzene 2: LDA / tetrahydrofuran 3: K2CO3 / methanol 4: aq. oxalic acid 5: NCS / CCl4 / 15 h / Ambient temperature 6: 90 percent / K2CO3 / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
De Kimpe, Norbert; Keppens, Marian; Fonck, Gwendolien
Chemical Communications, 1996 , # 5 p. 635 - 636
反应条件
trifluorormethanesulfonic acid T=5°C; 1 h;
参考文献
Yamazaki, Takahisa; Saito, Shin-ichi; Ohwada, Tomohiko; Shudo, Koichi
Tetrahedron Letters, 1995 , vol. 36, # 32 p. 5749 - 5752
反应条件
1: BF3*OEt2 / CH2Cl2 / 2 h / 0 °C 2: NaBH4 / ethanol / 3 h / 25 °C 3: 73 percent / TsCl, pyridine / DMAP / 1) 0 deg C, 15 min, 2) RT, 72h View Scheme
参考文献
Afonso; Barros; Godinho; Maycock
Synthesis, 1991 , # 7 p. 575 - 580
反应条件
lithium aluminium tetrahydride; oxygen T=110°C; P=759.8 Torr; 1.) oxidation, 2.) reductiv reactions of different α-diketones to different products; Product distribution;
参考文献
Rao, T. S. S.; Pritzkow, W.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 3 p. 474 - 482
反应条件
titanium(III) chloride in acetic acid T=50°C; 0.666667 h;
参考文献
Journal of Organic Chemistry, , vol. 56, # 24 p. 6813 - 6818
反应条件
titanium(III) chloride in acetic acid 0.666667 h;
参考文献
Journal of Organic Chemistry, , vol. 56, # 24 p. 6813 - 6818
反应条件
hydroxylamine hydrochloride
参考文献
Organic Letters, , vol. 13, # 13 p. 3388 - 3391
反应条件
ethanol; hydroxylamine hydrochloride; sodium carbonate
参考文献
Justus Liebigs Annalen der Chemie, , vol. 291, p. 267
反应条件
titanium(III) chloride in acetic acid 0.666667 h; Ambient temperature;
参考文献
Clerici, Angelo; Porta, Ombretta
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6813 - 6818
反应条件
titanium(III) chloride in acetic acid 0.666667 h;
参考文献
Clerici, Angelo; Porta, Ombretta
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6813 - 6818
