1-苯基-1,2-丙二酮合成路线 (共 223 条)
反应条件
1: 50 percent / diethyl ether / 0.5 h / Heating 2: oxygen; 5,10,15,20-tetraphenyl-21H,23H-porphine / acetonitrile / 6 h / Irradiation View Scheme
参考文献
Gollnick, Klaus; Koegler, Sigrid
Tetrahedron Letters, 1988 , vol. 29, # 10 p. 1127 - 1130
反应条件
indium; ammonium chloride in methanol 6 h; Heating;
参考文献
Kang, Suk-Ku; Baik, Tae-Gon; Jiao, Xiang-Hua
Synthetic Communications, 2002 , vol. 32, # 1 p. 75 - 78
反应条件
in acetonitrile T=20°C; 5 h; Inert atmospherePhotolysis;
参考文献
Nishigaichi, Yutaka; Suzuki, Akira; Takuwa, Akio
Tetrahedron Letters, 2007 , vol. 48, # 2 p. 211 - 214
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-5°C; also photochemical reaction without BF3*OEt2, other ketones, other stannanes; Product distribution;
参考文献
Takuwa, Akio; Nishigaichi, Yutaka; Yamashita, Koichi; Iwamoto, Hidetoshi
Chemistry Letters, 1990 , # 9 p. 1761 - 1764
反应条件
carbon monoxide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; selenium in tetrahydrofuran T=120°C; P=22800 Torr; 24 h;
参考文献
Tetrahedron Letters, , vol. 33, # 42 p. 6347 - 6350
反应条件
amberlyst-15 in water
T=70°C; 0.166667 h;
参考文献
Liu, Ju-Yan; Liu, Jing; Wang, Jia-Di; Jiao, De-Quan; Liu, Hai-Wang
Synthetic Communications, 2010 , vol. 40, # 14 p. 2047 - 2056
反应条件
sodium acetate; acetic acid
参考文献
v. Auwers
Chemische Berichte, 1917 , vol. 50, p. 1180
反应条件
trifluorormethanesulfonic acid
T=5°C; 1 h;
参考文献
Ohwada, Tomohiko; Yamazaki, Takahisa; Suzuki, Takayoshi; Saito, Shinichi; Shudo, Koichi
Journal of the American Chemical Society, 1996 , vol. 118, # 26 p. 6220 - 6224
反应条件
trifluorormethanesulfonic acid
T=5°C; 1 h;
参考文献
Yamazaki, Takahisa; Saito, Shin-ichi; Ohwada, Tomohiko; Shudo, Koichi
Tetrahedron Letters, 1995 , vol. 36, # 32 p. 5749 - 5752
反应条件
trifluorormethanesulfonic acid; trifluoroacetic acid
参考文献
Yamazaki, Takahisa; Saito, Shin-ichi; Ohwada, Tomohiko; Shudo, Koichi
Tetrahedron Letters, 1995 , vol. 36, # 32 p. 5749 - 5752