1-苯基-1,2-丙二酮合成路线 (共 223 条)
反应条件
methyltriphenylphosphonium tribromide; water 1.) THF, 48 h, room temperature; further reagents, solvents and times; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 27, # 26 p. 2965 - 2966
反应条件
ammonium cerium(IV) nitrate in acetonitrile T=20°C; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 12 p. 4516 - 4520
反应条件
2,2'-azo-bisisobutyronitrile; oxygen; palladium diacetate; sodium carbonate T=120°C; P=6080.41 Torr; 20 h; Autoclave;
参考文献
Journal of Organic Chemistry, , vol. 76, # 16 p. 6958 - 6961
反应条件
hydrogenchloride in acetone 2.5 h; Heating;
参考文献
Tetrahedron Letters, , vol. 24, # 23 p. 2361 - 2362
反应条件
potassium permanganate in water; acetone T=20°C; 2 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 3.2 p. 664 - 666
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 738 - 740
反应条件
CuCl2*2H2O in water; acetone Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 39, # 7 p. 1854 - 1856
反应条件
Oxonereg;; 2-iodo-3,4,5,6-tetramethylbenzoic acid in water; acetonitrile T=20°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 76, # 23 p. 9593 - 9601
反应条件
iodine; sodium acetate in tetrahydrofuran; water T=35°C; 3 h; IrradiationGreen chemistry;
参考文献
Journal of Organic Chemistry, , vol. 78, # 22 p. 11584 - 11589
反应条件
potassium permanganate; magnesium sulfate in toluene T=50 - 60°C; 40 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 101, # 1-4 p. 281 - 286
反应条件
dihydrogen peroxide; 1,5-dicyclohexyl imidazole; Mn(III)-salophen in dichloromethane; N,N-dimethyl-formamide T=0°C; 1.25 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 47, # 12 p. 1923 - 1926