1-苯基-1,2-丙二酮合成路线 （共 223 条）
反应条件
1: tetra-n-propylammonium perruthenate; N-methyl morpholine oxide / CH2Cl2 / 1 h / 25 °C 2: 93 percent / (tris(1-pyrazolyl)borate)RuPPh3(CH3CN)2PF6 / toluene / 5 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 8 p. 2793 - 2796
反应条件
1: m-chloroperbenzoic acid / CH2Cl2 2: tetra-n-propylammonium perruthenate; N-methyl morpholine oxide / CH2Cl2 / 1 h / 25 °C 3: 93 percent / (tris(1-pyrazolyl)borate)RuPPh3(CH3CN)2PF6 / toluene / 5 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 8 p. 2793 - 2796
反应条件
1: tetrahydrofuran / 2 h / 0 °C 2: m-chloroperbenzoic acid / CH2Cl2 3: tetra-n-propylammonium perruthenate; N-methyl morpholine oxide / CH2Cl2 / 1 h / 25 °C 4: 93 percent / (tris(1-pyrazolyl)borate)RuPPh3(CH3CN)2PF6 / toluene / 5 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 8 p. 2793 - 2796
反应条件
iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in water T=20°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 50, # 21 p. 2493 - 2496
反应条件
tert.-butylhydroperoxide; C3H7NO*C31H31Cl4Fe2N7O3 in acetonitrile T=60°C; 1 h;
参考文献
Inorganica Chimica Acta, , vol. 390, p. 129 - 134
反应条件
TDBPA(1+)*SbCl6(1-) in dichloromethane 0.25 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 34, # 24 p. 3897 - 3900
反应条件
acetaldehyde; 1,8-diazabicyclo[5.4.0]undec-7-ene T=0°C; 2.5 h; Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 8 p. 2368 - 2377
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=0°C; 2.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 8 p. 2368 - 2377
反应条件
in toluene T=110°C; 3 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 10 p. 3958 - 3961
反应条件
1: diethyl ether 2: CH3COOH / 16 h / Heating View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 115, # 1 p. 33 - 36
