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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
57901-65-2
合成路线
（共 8 条）
57901-63-0
→
反应条件
57901-65-2
反应条件
hydrogenchloride in tetrahydrofuran T=90°C; 4 h;
参考文献
Hassan, Abdalla E. A.; Wang, Peiyuan; McBrayer, Tamara; Tharnish, Philip; Stuyver, Lieven; Otto, Michael J.; Watanabe, Kyoichi A.; Schinazi, Raymond F.
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 10-12 p. 1531 - 1542
57901-59-4
→
反应条件
57901-65-2
反应条件
1: 79 percent / NaN3 / dimethylformamide / 72 h / 110 - 120 °C 2: 98 percent / hydrochloric acid / tetrahydrofuran / 4 h / 90 °C View Scheme
参考文献
Hassan, Abdalla E. A.; Wang, Peiyuan; McBrayer, Tamara; Tharnish, Philip; Stuyver, Lieven; Otto, Michael J.; Watanabe, Kyoichi A.; Schinazi, Raymond F.
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 10-12 p. 1531 - 1542
57901-60-7
→
反应条件
57901-65-2
反应条件
1: NaN3 / dimethylformamide / 5 h / 110 °C 2: ion exchange resin <H+-form> / methanol / Heating View Scheme
参考文献
Sasaki,T. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 1100 - 1104
909723-60-0
→
反应条件
57901-65-2
反应条件
1: NaN3 / dimethylformamide / 80 °C 2: dimethylformamide / 30 h / 110 - 120 °C 3: aq. HCl / tetrahydrofuran / 90 °C View Scheme
参考文献
Hassan, Abdalla E. A.; Wang, Peiyuan; McBrayer, Tamara R.; Tharnish, Phillip M.; Stuyver, Lieven J.; Schinazi, Raymond F.; Otto, Michael J.; Watanabe, Kyoichi A.
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 5-7 p. 961 - 964
57901-66-3
→
反应条件
57901-65-2
反应条件
1: dimethylformamide / 30 h / 110 - 120 °C 2: aq. HCl / tetrahydrofuran / 90 °C View Scheme
参考文献
Hassan, Abdalla E. A.; Wang, Peiyuan; McBrayer, Tamara R.; Tharnish, Phillip M.; Stuyver, Lieven J.; Schinazi, Raymond F.; Otto, Michael J.; Watanabe, Kyoichi A.
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 5-7 p. 961 - 964
957-75-5
5-溴尿苷
→
反应条件
57901-65-2
反应条件
1: 94 percent / HCl / diethyl ether / 48 h / 20 °C 2: 87 percent / pyridine / 1 h / 20 °C 3: 76.7 percent / NaN3 / dimethylformamide / 120 h / 110 - 120 °C 4: 98 percent / hydrochloric acid / tetrahydrofuran / 4 h / 90 °C View Scheme
参考文献
Hassan, Abdalla E. A.; Wang, Peiyuan; McBrayer, Tamara; Tharnish, Philip; Stuyver, Lieven; Otto, Michael J.; Watanabe, Kyoichi A.; Schinazi, Raymond F.
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 10-12 p. 1531 - 1542
54503-61-6
5-溴-2',3'-O-异亚丙基尿苷
→
反应条件
57901-65-2
反应条件
1: 87 percent / pyridine / 1 h / 20 °C 2: 76.7 percent / NaN3 / dimethylformamide / 120 h / 110 - 120 °C 3: 98 percent / hydrochloric acid / tetrahydrofuran / 4 h / 90 °C View Scheme
参考文献
Hassan, Abdalla E. A.; Wang, Peiyuan; McBrayer, Tamara; Tharnish, Philip; Stuyver, Lieven; Otto, Michael J.; Watanabe, Kyoichi A.; Schinazi, Raymond F.
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 10-12 p. 1531 - 1542
656808-46-7
→
反应条件
57901-65-2
反应条件
1: 76.7 percent / NaN3 / dimethylformamide / 120 h / 110 - 120 °C 2: 98 percent / hydrochloric acid / tetrahydrofuran / 4 h / 90 °C View Scheme
参考文献
Hassan, Abdalla E. A.; Wang, Peiyuan; McBrayer, Tamara; Tharnish, Philip; Stuyver, Lieven; Otto, Michael J.; Watanabe, Kyoichi A.; Schinazi, Raymond F.
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 10-12 p. 1531 - 1542
