反应条件
anhydrous trisodium citrate in water CaCl2 soln. added to sodium citrate soln., stirred at 23°C; sodium oxalate soln. added, stirred for 10-15 min (or sodium oxalate soln. added rapidly to mixt. of CaCl2 soln. and sodium citrate soln.; stirred for 10 min at 23°C); ppt. filtered off; washed repeatedly with distilled water; dried to constant weight at ambient temp. over CaCl2 and in vac.; DTA; SEM;
参考文献
Crystal Research and Technology, , vol. 29, p. 517 - 524