2,4,6-三(吡咯烷-1-基)-1,3,5-三嗪合成路线 (共 5 条)
反应条件
trifluoromethylsulfonic anhydride in dichloromethane
T=20°C; 12 h;
参考文献
Herrera, Antonio; Martinez-Alvarez, Roberto; Ramiro, Pedro; Chioua, Mourad; Chioua, Rachid
Synthesis, 2004 , # 4 p. 503 - 505
反应条件
in dichloromethane
T=0°C;
参考文献
Kolesinska, Beata; Kaminski, Zbigniew J.
Tetrahedron, 2009 , vol. 65, # 18 p. 3573 - 3576
反应条件
T=160°C; P=3000240 Torr; 20 h;
参考文献
Shibuya, Isao; Oishi, Akihiro; Yasumoto, Masahiko
Heterocycles, 1998 , vol. 48, # 8 p. 1659 - 1662
参考文献
Detweiler; Amstutz
Journal of the American Chemical Society, 1952 , vol. 74, p. 1483
反应条件
chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane; mercury dichloride
1) heating, 2) reflux, 7 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad
Chemische Berichte, 1984 , vol. 117, # 4 p. 1523 - 1541