1-(乙酰氨基)-1-苯乙烯合成路线 (共 32 条)
反应条件
triethylamine in benzene
36 h;
参考文献
Padwa, Albert; Akiba, Mitsuo; Cohen, Leslie A.; MacDonald, Gavin J.
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 695 - 703
反应条件
1: methylmagnesium bromide; benzonitrile in diethyl ether
8 h; Heating;
2: acetic anhydride in diethyl ether
8 h; Heating;
参考文献
Enthaler, Stephan; Hagemann, Bernhard; Junge, Kathrin; Erre, Giulia; Beller, Matthias
European Journal of Organic Chemistry, 2006 , # 13 p. 2912 - 2917
反应条件
1: 100 percent / benzene / 5 h / Irradiation
2: 51 percent / triethylamine / benzene / 36 h
View Scheme
参考文献
Padwa, Albert; Akiba, Mitsuo; Cohen, Leslie A.; MacDonald, Gavin J.
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 695 - 703
反应条件
ozone; triethylamine
参考文献
Toshimitsu, Akio; Hayashi, Gen; Terao, Keiji; Uemura, Sakae
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2113 - 2118
反应条件
copper(l) iodide; potassium iodide in ethylenediamine
T=120°C; Inert atmosphere;
参考文献
Liang, Hao; Ren, Zhi-Hui; Wang, Yao-Yu; Guan, Zheng-Hui
Chemistry - A European Journal, 2013 , vol. 19, # 30 p. 9789 - 9794
反应条件
styrene; tetraethylammonium bromide in acetonitrile
electrolysis; Yield given;
参考文献
Knittel, Dierk
Monatshefte fuer Chemie, 1984 , vol. 115, p. 523 - 532
反应条件
1: potassium iodide; copper(l) iodide / ethylenediamine / 120 °C / |Inert atmosphere
2: triethylamine; palladium diacetate / N,N-dimethyl-formamide / 60 °C
View Scheme
参考文献
Liang, Hao; Ren, Zhi-Hui; Wang, Yao-Yu; Guan, Zheng-Hui
Chemistry - A European Journal, 2013 , vol. 19, # 30 p. 9789 - 9794
反应条件
1: 91 percent / trifluoromethanesulphonic acid, water / 1 h / Heating
2: 76 percent / ozone, triethylamine
View Scheme
参考文献
Toshimitsu, Akio; Hayashi, Gen; Terao, Keiji; Uemura, Sakae
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2113 - 2118
反应条件
1: 87 percent / trifluoromethanesulphonic acid, water / 10 h / Heating
2: 76 percent / ozone, triethylamine
View Scheme
参考文献
Toshimitsu, Akio; Hayashi, Gen; Terao, Keiji; Uemura, Sakae
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2113 - 2118
参考文献
Padwa, Albert; Akiba, Mitsuo; Cohen, Leslie A.; MacDonald, J. Gavin
Tetrahedron Letters, 1981 , vol. 22, # 26 p. 2435 - 2438