双(三甲基硅基)过氧化物合成路线 (共 69 条)
反应条件
in diethyl ether; hexane 3 h; Ambient temperature;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
in diethyl ether 2 h; Ambient temperature;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
n-butyllithium 1.) ether, room temp., 0.25 h, 2.) room temp., 3 h; Yield given. Multistep reaction;
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran T=-78°C;
参考文献
Tetrahedron Letters, , vol. 34, # 19 p. 3141 - 3144
反应条件
in diethyl ether T=-78°C;
参考文献
Tetrahedron, , vol. 44, # 13 p. 4197 - 4206
参考文献
Tetrahedron, , vol. 44, # 13 p. 4197 - 4206
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-78°C; 2 h; alkylation of other heteroaryl alkyl metals;
参考文献
Epifani, Erbana; Florio, Saverio; Troisi, Luigino
Tetrahedron, 1990 , vol. 46, p. 4031 - 4038
反应条件
in tetrahydrofuran; diethyl ether T=0°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
n-butyllithium 1.) ether, room temp., 0.33 h, 2.) room temp., 3 h; Yield given. Multistep reaction;
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
反应条件
in diethyl ether T=-78°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206