双(三甲基硅基)过氧化物合成路线 (共 69 条)
反应条件
in diethyl ether Ambient temperature-78 deg C to room temp.;
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
反应条件
in diethyl ether; hexane T=10°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
in diethyl ether Ambient temperature-78 deg C to room temp.;
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
参考文献
Brandes,D.; Blaschette,A.
Journal of Organometallic Chemistry, 1974 , vol. 73, p. 217 - 227
反应条件
lithium diisopropyl amide 1.1) Et2O, -78 deg C to room temp., 1.2) 40 min, reflux, 2.) -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Dembech; Guerrini; Ricci; Seconi; Taddei
Tetrahedron, 1990 , vol. 46, # 8 p. 2999 - 3006
反应条件
in dichloromethane; water
参考文献
Bender, Steven Lee; Bhumralkar, Dilip; Collins, Michael Raymond; Cripps, Stephen James; Deal, Judith Gail; Jia, Lei; Nambu, Mitchell David; Palmer, Cynthia Louise; Peng, Zhengwei; Varney, Michael David
Patent: US2002/103203 A1, 2002 ;
参考文献
Kowalski, Jozef; Wozniak, Lucyna; Chojnowski, Julian
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 30, p. 125 - 128
反应条件
lithium bromide in tetrahydrofuran; diethyl ether
T=0°C; Yield given. Yields of byproduct given;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
n-butyllithium
1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Florio, S.; Troisi, L.
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3721 - 3724
反应条件
n-butyllithium
1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Florio, S.; Troisi, L.
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3721 - 3724