反应条件
1.1: Zn; TMSCl; 1,2-dibromoethane / tetrahydrofuran / 30 °C 1.2: 80 percent / 5 percent Ni/C / toluene; dimethylformamide; tetrahydrofuran / 30 h / 20 °C 2.1: 92 percent / H2 / Pd(OH)2/C / ethyl acetate / 6 h / 30 °C / 3040 Torr 3.1: aq. HBr / toluene / 40 h / Heating 4.1: 22 g / aq. NaOH / toluene; methoxybenzene / 6 h / 30 °C View Scheme