反应条件
1: LiN3 / dimethylformamide / 2.5 h / 130 °C 2: H2 / Pd-C / ethanol / 16 h / 25 °C / 2327.2 Torr 3: (i) aq. Ba(OH)2, (ii) /BRN= 1098367/, (iii) /BRN= 1098229/, H2SO4 4: LiBH4 / tetrahydrofuran / 3.5 h / Heating 5: HBr / acetic acid / 0.5 h / 100 °C 6: (i) Na, (ii) /BRN= 4047078/, (iii) aq. Ba(OH)2, MeOH 7: aq. NaOH / 0.5 h / 180 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 99, p. 7020 - 7026
