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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴代萘
合成路线
（共 389 条）
1809-10-5
3-溴戊烷
+
580-13-2
2-溴代萘
→
反应条件
3042-57-7
反应条件
1: 2-bromo-naphthalene With iodine; magnesium in tetrahydrofuran T=60°C; Inert atmosphereReflux; 2: 3-pentyl bromide With (FeCl3)2(TMEDA)3 in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Luan, Xinjun; Wu, Linglin; Drinkel, Emma; Mariz, Ronaldo; Gatti, Michele; Dorta, Reto
Organic Letters, 2010 , vol. 12, # 9 p. 1912 - 1915
580-13-2
2-溴代萘
→
反应条件
2579-21-7
4,4-二甲基-2-戊炔醛
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 10 h;
参考文献
Oh, Chang Ho; Jung, Seung Hyun; Bang, Su Youn; Park, Dai In
Organic Letters, 2002 , vol. 4, # 19 p. 3325 - 3327
580-13-2
2-溴代萘
→
反应条件
239-30-5
苯并[b]萘并[2,1-d]呋喃
+
1400967-84-1
反应条件
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / methanol; toluene / 24 h / |Reflux 2: boron tribromide / dichloromethane / 0 - 20 °C / |Inert atmosphere 3: water / acetonitrile / 1 h / |Inert atmosphere; |UV-irradiation View Scheme
参考文献
Basaric, Nikola; Doslic, Nacrossed D Signa; Ivkovic, Jakov; Wang, Yu-Hsuan; Veljkovic, Jelena; Mlinaric-Majerski, Kata; Wan, Peter
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1811 - 1823
580-13-2
2-溴代萘
→
反应条件
23992-63-4
反应条件
1.1: tris-(dibenzylideneacetone)dipalladium(0); PtBu3; lithium hexamethyldisilazane / Inert atmosphere 1.2: Inert atmosphere 2.1: BTEAICl2 / methanol; dichloromethane / Inert atmosphere 3.1: boron trifluoride diethyl etherate / tetrahydrofuran / 0.08 h / -15 - -10 °C / Inert atmosphere 3.2: 0.5 h / -15 - 5 °C / Inert atmosphere 3.3: 2 h / 20 °C / Inert atmosphere 4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / tetrahydrofuran / 0.75 h / 20 °C / Inert atmosphere 4.2: 20 °C / Inert atmosphere 5.1: methanol; potassium carbonate / tetrahydrofuran / 20 °C / Inert atmosphere 6.1: 1,2-dichloro-benzene / 200 °C View Scheme
参考文献
McClintock, Sean P.; Zakharov, Lev N.; Herges, Rainer; Haley, Michael M.
Chemistry - A European Journal, 2011 , vol. 17, # 24 p. 6798 - 6806
580-13-2
2-溴代萘
+
106-96-7
3-溴丙炔
→
反应条件
25033-18-5
反应条件
1: propargyl bromide With 9-borabicyclo[3.3.1]nonane dimer in tetrahydrofuran dihydroboration; 2 h; Heating; 2: With sodium hydroxide in tetrahydrofuran T=20°C; Hydrolysis; 1 h; 3: 2-bromo-naphthalene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=65°C; Suzuki-Miyaura coupling; 8 h;
参考文献
Soderquist, John A.; Huertas, Ramon; Leon-Colon, Gisela
Tetrahedron Letters, 2000 , vol. 41, # 22 p. 4251 - 4255
580-13-2
2-溴代萘
+
3002-94-6
→
反应条件
25033-18-5
反应条件
Pd0(tris(tert-butyl)phosphine)2 in toluene T=20°C; 1 h;
参考文献
Vila, Carlos; Giannerini, Massimo; Hornillos, Valentin; Fananas-Mastral, Martin; Feringa, Ben L.
Chemical Science, 2014 , vol. 5, # 4 p. 1361 - 1367
580-13-2
2-溴代萘
+
108-91-8
环己胺
→
反应条件
23761-52-6
N-环己基-2-萘胺
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium (0) in toluene T=105 - 110°C; 16 h;
参考文献
Kwit; Gawronski
Tetrahedron, 2003 , vol. 59, # 47 p. 9323 - 9331
580-13-2
2-溴代萘
+
7664-41-7
氨气
→
反应条件
134-32-7
1-萘胺
+
91-59-8
2-萘胺
反应条件
T=-33°C;
参考文献
Urner; Bergstrom
Journal of the American Chemical Society, 1945 , vol. 67, p. 2108
580-13-2
2-溴代萘
+
201230-82-2
→
反应条件
2459-25-8
+
93-09-4
反应条件
methanol; 1,1-dimethylpropan-1-ol; sodium hydride; anhydrous cobalt diacetate in tetrahydrofuran T=40°C; P=760 Torr; 85 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 60, # 26 p. 8336 - 8340
67-56-1
+
580-13-2
2-溴代萘
+
68-12-2
→
反应条件
13577-85-0
+
2459-25-8
反应条件
1: 2-bromo-naphthalene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Tetrahedron, , vol. 68, # 24 p. 4701 - 4709
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