2,4,6-三苯基吡啶合成路线 (共 217 条)
反应条件
1: With [Hmim][NO3]; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=96°C; Ionic liquidMicrowave irradiation; 2: With ammonium acetate T=96°C; 0.136111 h; Ionic liquidMicrowave irradiation;
参考文献
Khosropour, Ahmad R.; Mohammadpoor-Baltork, Iraj; Kiani, Forough
Comptes Rendus Chimie, 2011 , vol. 14, # 5 p. 441 - 445
反应条件
1: benzyl alcohol With [Hmim][NO3]; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=96°C; 0.0555556 h; Ionic liquidMicrowave irradiation; 2: acetophenone With ammonium acetate T=96°C; 0.111111 h; Ionic liquidMicrowave irradiation;
参考文献
Khosropour, Ahmad R.; Mohammadpoor-Baltork, Iraj; Kiani, Forough
Comptes Rendus Chimie, 2011 , vol. 14, # 5 p. 441 - 445
反应条件
1: With tetrakis(triphenylphosphine) palladium(0); sodium acetate in N,N-dimethyl-formamide T=80°C; 12 h; Inert atmosphere; 2: in N,N-dimethyl-formamide T=80°C; 12 h; Reagent/catalyst;
参考文献
Organic Letters, , vol. 15, # 2 p. 334 - 337
反应条件
in ethanol T=80°C; 8 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 19, # 4 p. 741 - 745
反应条件
ammonium acetate in acetic acid T=100°C; 1 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 22, # 10 p. 1068 - 1071
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 22, # 10 p. 1321 - 1324
反应条件
ammonium acetate in acetic acid 6 h; Heating;
参考文献
Tewari, Ram S.; Awasthi, Alok K.
Synthesis, 1981 , # 4 p. 314 - 315
反应条件
hydrogen; nickel ruthenium in methanol T=100°C; P=7598.1 Torr; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 20, # 12 p. 1361 - 1364
Khimiya Geterotsiklicheskikh Soedinenii, , # 12 p. 1652 - 1655
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in toluene T=130°C; 24 h; Inert atmosphere;
参考文献
Ohashi, Masato; Takeda, Ippei; Ikawa, Masashi; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18018 - 18021
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate) T=100°C; 20 h; Sealed tube;
参考文献
Huang, Huawen; Ji, Xiaochen; Wu, Wanqing; Huang, Liangbin; Jiang, Huanfeng
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3774 - 3782
反应条件
ammonium acetate in acetic acid 1.) reflux, 8 h, 2.) overnight, room temp.;
参考文献
Tewari, Ram. S.; Dubey, Ajay K.; Misra, Naresh K.; Dixit, Priya D.
Journal of Chemical & Engineering Data, 1981 , vol. 26, # 1 p. 106 - 108