2,4,6-三苯基吡啶合成路线 (共 217 条)
反应条件
ammonium acetate in acetic acid 3 h; Heating;
参考文献
Tewari, R. S.; Dubey, A. K.
Journal of Chemical & Engineering Data, 1980 , vol. 25, # 1 p. 91 - 92
反应条件
1: With sodium hydroxide; hydroxylamine hydrochloride in diethyl ether Ring cleavage; 0.25 h; 2: With phosphorus pentachloride in diethyl ether T=0°C; Beckmann reaction; 0.333333 h;
参考文献
Tetrahedron, , vol. 55, # 52 p. 15011 - 15024
反应条件
ammonium acetate in methanol 4 h; Reflux;
参考文献
Shinpuku, Yoshiki; Inui, Fumiaki; Nakai, Misaki; Nakabayashi, Yasuo
Journal of Photochemistry and Photobiology A: Chemistry, 2011 , vol. 222, # 1 p. 203 - 209
反应条件
1: With boron trifluoride diethyl etherate; lithium chloride in tetrahydrofuran T=-78°C; 0.5 h; 2: in tetrahydrofuran T=20°C; 3 h;
参考文献
Abdel-Aziz, Alaa A.-M.
Tetrahedron Letters, 2007 , vol. 48, # 16 p. 2861 - 2865
反应条件
1: 56 percent / NEt3 / CH2Cl2; petroleum ether / 1) -40 deg C, 60 min, 2) -40 deg C to RT, 60 min 2: 1) t-BuOK / 1) benzene, RT, 5 min, 2) 24h View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 7 p. 1937 - 1942
反应条件
1: boron fluoride ether adduct 2: aqueous ammonia View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 1458,1460
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate) T=100°C; 20 h; Sealed tube;
参考文献
Huang, Huawen; Ji, Xiaochen; Wu, Wanqing; Huang, Liangbin; Jiang, Huanfeng
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3774 - 3782
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate) T=100°C; 20 h; Sealed tube;
参考文献
Huang, Huawen; Ji, Xiaochen; Wu, Wanqing; Huang, Liangbin; Jiang, Huanfeng
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3774 - 3782
反应条件
in water T=90°C; 20 h;
参考文献
Katritzky, Alan R.; Rubio, Olga
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4017 - 4021
反应条件
DPAT T=120°C; 4.5 h; Neat (no solvent); regioselective reaction;
参考文献
Tetrahedron, , vol. 68, # 22 p. 4138 - 4144