2,4,6-三苯基吡啶合成路线 （共 217 条）
反应条件
hexafluoroisopropyl alcohol T=180°C; 43 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 4 p. 325 - 327
反应条件
1: 25 percent / BF3-OEt2 / 0.5 h / 100 °C 2: NH3 / ethanol / 0.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 125 - 130
反应条件
1: BF3-Et2O 2: NH3 / ethanol / 0.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 125 - 130
反应条件
1: HCl / ethanol / 0.17 h / Heating 2: 70 percent / ammonium acetate / acetic acid; ethanol / 2 h / Heating 3: 34 percent / ethanol / 1.67 h / Irradiation View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1607 - 1612
反应条件
1: 70 percent / ammonium acetate / acetic acid; ethanol / 2 h / Heating 2: 34 percent / ethanol / 1.67 h / Irradiation View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1607 - 1612
反应条件
1: K2CO3 / benzene 2: 92 percent / NaN3, tetrabutylammoniumsulfate / CHCl3; H2O / 72 h / Heating 3: methanol / Irradiation; various solvents; influence of wavelenght on kind of products View Scheme
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 28, # 5 p. 189 - 190
反应条件
1: 92 percent / NaN3, tetrabutylammoniumsulfate / CHCl3; H2O / 72 h / Heating 2: methanol / Irradiation; various solvents; influence of wavelenght on kind of products View Scheme
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 28, # 5 p. 189 - 190
反应条件
1: 13 percent / diethyl ether / 4 h / Ambient temperature 2: 7 percent / silica gel / benzene / 72 h / Ambient temperature View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 494 - 500
反应条件
1: 40 percent / Sodium hydride / diethyl ether / 4 h 2: 0.2 g / Ammonium acetate / acetic acid / 1 h / 100 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 22, # 10 p. 1068 - 1071
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 22, # 10 p. 1321 - 1324
反应条件
1: 52 percent / NaOH / ethanol / 26 h / 20 °C 2: 0.2 g / Ammonium acetate / acetic acid / 1 h / 100 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 22, # 10 p. 1068 - 1071
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 22, # 10 p. 1321 - 1324
