N-(2-吡啶基甲基)-1-丁胺合成路线 （共 8 条）
反应条件
sodium tetrahydroborate in ethanol
1) -10 deg C, 2 h 2) r.t., 3 h;
参考文献
Brunner; Nerl; Angerer; Knebel
Archiv der Pharmazie, 1991 , vol. 324, # 10 p. 779 - 784
反应条件
η5-cyclopentadienyl-η4-cycloocta-1,5-diene-cobalt(I) in toluene
T=25°C; Irradiation;
参考文献
Heller, Barbara; Sundermann, Bernd; Buschmann, Helmut; Drexler, Hans-Joachim; You, Jingsong; Holzgrabe, Ulrike; Heller, Eberhard; Oehme, Guenther
Journal of Organic Chemistry, 2002 , vol. 67, # 13 p. 4414 - 4422
反应条件
1: CH2Cl2 / 24 h / 20 °C
2: 2.95 g / Na2SO4 / CH2Cl2 / 24 h / 20 °C
3: aq. H2SO4 / 2 h / 95 - 100 °C
View Scheme
参考文献
Goldeman, Waldemar; Olszewski, Tomasz K.; Boduszek, Bogdan; Sawka-Dobrowolska, Wanda
Tetrahedron, 2006 , vol. 62, # 18 p. 4506 - 4518
反应条件
hydrogenchloride
6 h; Heating;
参考文献
Boduszek, Bogdan
Tetrahedron, 1996 , vol. 52, # 38 p. 12483 - 12494
反应条件
sulfuric acid
T=95 - 100°C; 2 h;
参考文献
Goldeman, Waldemar; Olszewski, Tomasz K.; Boduszek, Bogdan; Sawka-Dobrowolska, Wanda
Tetrahedron, 2006 , vol. 62, # 18 p. 4506 - 4518
反应条件
sulfuric acid
T=20°C;
参考文献
Boduszek, Bogdan; Olszewski, Tomasz; Goldeman, Waldemar; Konieczna, Magdalena
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 4 p. 787 - 795
反应条件
hydrogenchloride
6 h; Heating;
参考文献
Boduszek, Bogdan
Tetrahedron, 1996 , vol. 52, # 38 p. 12483 - 12494
反应条件
sulfuric acid in methanol
T=25°C; Kinetics; Further Variations:concentrations of reagent;
参考文献
Boduszek, Bogdan; Olszewski, Tomasz; Goldeman, Waldemar; Konieczna, Magdalena
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 4 p. 787 - 795
