2,2’-联苯二甲酸乙酯合成路线 （共 13 条）
反应条件
1: With isopropylmagnesium chloride in tetrahydrofuran T=-20°C; 0.166667 h; 2: With copper(I) bromide dimethylsulfide complex in tetrahydrofuran T=-20°C; 0.00833333 h; 3: With (3,5-dinitrophenyl)(4-methylpiperazin-1-yl)methanone in tetrahydrofuran T=-20 - 20°C;
参考文献
Surry, David S.; Su, Xianbin; Fox, David J.; Franckevicius, Vilius; Macdonald, Simon J. F.; Spring, David R.
Angewandte Chemie - International Edition, 2005 , vol. 44, # 12 p. 1870 - 1873
反应条件
1: With zinc in tetrahydrofuran Heating; 2: With (3,5-dinitrophenyl)(4-methylpiperazin-1-yl)methanone; copper(I) bromide dimethylsulfide complex in N,N-dimethyl acetamide T=22°C; 1 h;
参考文献
Moncomble, Aurelien; Floch, Pascal Le; Gosmini, Corinne
Chemistry - A European Journal, 2009 , vol. 15, # 19 p. 4770 - 4774
反应条件
3,3',5,5'-tetra-tert-butyl-4,4'-diphenoquinone; lithium chloride in tetrahydrofuran
参考文献
Krasovskiy, Arkady; Tishkov, Alexander; Del Amo, Vicente; Mayr, Herbert; Knochel, Paul
Angewandte Chemie - International Edition, 2006 , vol. 45, # 30 p. 5010 - 5014
反应条件
sulfuric acid 3 h; Heating;
参考文献
Steliou, Kosta; Salama, Paul; Yu, Xiaoping
Journal of the American Chemical Society, 1992 , vol. 114, # 4 p. 1456 - 1462
反应条件
tetrabutyl-ammonium chloride; palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=110°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 49, # 46 p. 6569 - 6572
参考文献
Tetrahedron, , vol. 31, p. 2029 - 2039
反应条件
1: diethyl ether 2: 200 °C View Scheme
参考文献
Tetrahedron, , vol. 31, p. 2029 - 2039
参考文献
Yuki Gosei Kagaku Kyokaishi, , vol. 17, p. 91
Chem.Abstr., , p. 8058
参考文献
Canadian Journal of Chemistry, , vol. 30, p. 208,221
反应条件
1: LiAlH4 2: aqueous HBr 3: magnesium; diethyl ether View Scheme
参考文献
Hall et al.
Journal of the Chemical Society, 1950 , p. 711
