(C4H9)4NClO4 in ethylene glycol dimethyl ether Electrolysis; exhaustive controlled potential electrolysis on plateau of oxdn. wave at 25°C in anhyd., deoxygenated DME; not isolated, detected by voltammetric, IR, and polarographic measurements of final anolite;

(C4H9)4NClO4 in 1,2-dichloro-ethane Electrolysis; exhaustive controlled potential electrolysis on plateau of oxdn. wave in CH2ClCH2Cl; not isolated, detected by voltammetric, IR, and polarographic measurements of final anolite;