N-[二(甲硫基)亚甲基]甘氨酸甲酯合成路线 (共 6 条)
反应条件
1: carbon disulfide; (benzhydrylideneamino)acetic acid methyl ester With triethylamine in dichloromethane T=20°C; 0.5 h; 2: methyl iodide With triethylamine in dichloromethane Heating;
参考文献
Krishnaswamy; Govande; Gumaste; Bhawal; Deshmukh
Tetrahedron, 2002 , vol. 58, # 11 p. 2215 - 2225
反应条件
potassium carbonate in tetrahydrofuran
参考文献
The Journal of organic chemistry, , vol. 41, # 7 p. 1112 - 1117
反应条件
potassium carbonate in acetone Heating;
参考文献
Tetrahedron, , vol. 49, # 2 p. 497 - 506
反应条件
triethylamine 1) methylene chloride, room temperature, 30 min, 2) a) reflux, 3 h, b) reflux, 4 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 49, # 10 p. 2101 - 2108
反应条件
in tetrahydrofuran T=30°C; 6 h;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 11 p. 1623 - 1627
参考文献
Garner, Philip; Dogan, Oezdemir; Youngs, Wiley J.; Kennedy, Vance O.; Protasiewicz, John; Zaniewski, Rebecca
Tetrahedron, 2001 , vol. 57, # 1 p. 71 - 85