3-环戊烯-1-甲酸甲酯合成路线 （共 15 条）
反应条件
1: 3-cyclopentene-1-carboxylic acid With 1,1'-carbonyldiimidazole in dichloromethane T=0 - 20°C; 4 h; 2: methanol in dichloromethane
参考文献
Wang, Yuguang; Chackalamannil, Samuel; Root, Yuriko Y.
Patent: US2007/254952 A1, 2007 ;
Location in patent: Page/Page column 35 ;
US 20070254952 A1
反应条件
potassium carbonate in DMF (N,N-dimethyl-formamide) T=20°C; 16 h;
参考文献
Butora, Gabor; Goble, Stephen D.; Pastemak, Alexander; Yang, Lihu; Zhou, Changyou; Moyes, Christopher R.
Patent: US2008/81803 A1, 2008 ;
Location in patent: Page/Page column 35 ;
US 20080081803 A1
反应条件
lithium chloride in dimethyl sulfoxide T=150°C; 3 h;
参考文献
Wainwright, Phillip; Maddaford, Adrian; Bissell, Richard; Fisher, Ray; Leese, David; Lund, Andrew; Runcie, Karen; Dragovich, Peter S.; Gonzalez, Javier; Kung, Pei-Pei; Middleton, Donald S.; Pryde, David C.; Stephenson, Peter T.; Sutton, Scott C.
Synlett, 2005 , # 5 art. no. D36004ST, p. 765 - 768
反应条件
tetramethyl-1,1,3,3 disila-1,3 cyclobutane; tungsten hexachloride in benzene T=80°C; P=0.001 Torr; 10 h;
参考文献
Russian Chemical Bulletin, , vol. 43, # 8 p. 1425 - 1426
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , # 8 p. 1503 - 1504
反应条件
hydrogenchloride; potassium hydroxide in methanol; water
参考文献
EP339669 A1, ;
EP 0339669 A1
反应条件
methanesulfonic acid; oxygen; palladium diacetate; NPMoV T=50°C; P=760 Torr; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 67, # 14 p. 5005 - 5008
参考文献
Lizotte, Kathryn E.; Marecki, Paul E.; Mertes, Mathias P.
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3594 - 3597
反应条件
1: 93 percent / Grubbs' catalyst / CH2Cl2 / 72 h / Heating 2: 78 percent / LiCl / dimethylsulfoxide / 3 h / 150 °C View Scheme
参考文献
Synlett, , # 5 art. no. D36004ST, p. 765 - 768
反应条件
1: C26H34N5O2Pol With Grubb's 2nd generation catalyst in dichloromethane T=20°C; 24 h; solid phase reaction; 2: methanol With copper(II) bis(trifluoromethanesulfonate) T=20°C; 15 h; solid phase reaction;
参考文献
Kramer, Rolf A.; Broehmer, Manuel C.; Forkel, Nina V.; Bannwarth
European Journal of Organic Chemistry, 2009 , # 25 p. 4273 - 4283
反应条件
1: SOCl2 / toluene / Heating 2: CH2Cl2 View Scheme
参考文献
Synthetic Communications, , vol. 22, # 22 p. 3197 - 3204
