1,1,3,3,3-五氟-2-(氟甲氧基)-1-丙烯合成路线 (共 2 条)
反应条件
methyllithium in formaldehyde diethyl acetal
T=-31 - -20°C; Inert atmosphere; Product distribution / selectivity;
参考文献
BAXTER INTERNATIONAL INC.; BAXTER HEALTHCARE S.A.
Patent: US2010/267995 A1, 2010 ;
Location in patent: Page/Page column 3-4 ;
反应条件
soda lime
T=120°C; 0.666667 h; further time and temperature; also with D2-sevoflurane; Product distributionMechanism;
参考文献
Ruzicka, Jan A.; Baker, Max T.
Journal of Fluorine Chemistry, 1995 , vol. 71, # 1 p. 55 - 58