1-(2,4-二羟基-5-甲氧基苯基)-2-(4-羟基苯基)-3,3-二甲氧基-1-丙酮合成路线 （共 5 条）
反应条件
hydrogenchloride in methanol; water Heating / reflux;
参考文献
THE UNIVERSITY COURT OF THE UNIVERSITY OF ST ANDREWS
Patent: WO2004/69774 A2, 2004 ;
Location in patent: Page 89 ;
反应条件
1: 70 percent / conc. aq. HCl / methanol / 0.25 h / Heating 2: 17 percent / silver oxide, pyridine / 1.) 15 min, 2.) 2.5 h 3: 70 percent / NaOMe / 0.33 h / Heating View Scheme
参考文献
Nogradi, Mihaly; Szoellosy, Aron
Liebigs Annales, 1996 , # 10 p. 1651 - 1652
反应条件
hydrogen; 5-palladium/activated carbon in methanol; acetone
T=20°C; 12 h;
参考文献
THE UNIVERSITY COURT OF THE UNIVERSITY OF ST ANDREWS
Patent: WO2004/69774 A2, 2004 ;
Location in patent: Page 89 ;
反应条件
hydrogen; palladium on activated charcoal in methanol; acetone
参考文献
Nogradi, Mihaly; Szoellosy, Aron
Liebigs Annales, 1996 , # 10 p. 1651 - 1652
反应条件
1: 91 percent / 50percent aq. NaOH / ethanol / 1 h / Heating
2: 90 percent / Tl(NO3)3*3H2O / methanol / 1 h
3: 95 percent / H2 / Pd/C / methanol; acetone
View Scheme
参考文献
Nogradi, Mihaly; Szoellosy, Aron
Liebigs Annales, 1996 , # 10 p. 1651 - 1652
