3-(3-氯苯基)-1-苯基-1-丙酮合成路线 (共 5 条)
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; silica gel in toluene
T=70°C; 17 h; Inert atmosphereDarkness;
参考文献
Stroba, Adriana; Schaeffer, Francis; Hindie, Valerie; Lopez-Garcia, Laura; Adrian, Iris; Froehner, Wolfgang; Hartmann, Rolf W.; Biondi, Ricardo M.; Engel, Matthias
Journal of Medicinal Chemistry, 2009 , vol. 52, # 15 p. 4683 - 4693
反应条件
C29H38ClIrN2; potassium hydroxide in toluene
T=100°C; 6 h; Sealed tube;
参考文献
Segarra, Candela; Mas-Marza, Elena; Mata, Jose A.; Peris, Eduardo
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2078 - 2084
反应条件
sodium hydrogen telluride in ethanol; N,N-dimethyl-formamide
3 h; Ambient temperature;
参考文献
Huang, Xian; Zhang, Han-zhong
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 97 - 106
反应条件
tetrachlorosilane; sodium iodide in acetonitrile
0.5 h; Ambient temperature;
参考文献
Elmorsy, Saad S.; El-Ahl, Abdel-Aziz S.; Soliman, Hanan; Amer, Fathy A.
Tetrahedron Letters, 1996 , vol. 37, # 13 p. 2297 - 2298
反应条件
sodium hydrogen telluride in ethanol; N,N-dimethyl-formamide
4 h; Ambient temperature;
参考文献
Huang, Xian; Zhang, Han-zhong
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 97 - 106