反应条件
in dichloromethane
6 mmol of the Sb compound suspended in CH2Cl2; addn. of 12 mmol Me2S2 i CH2Cl2 at -65°C; ppt. filtered off at -65°C, washed with CH2Cl2, and dried;
参考文献
Minkwitz, R.; Gerhard, V.; Krause, R.; Prenzel, H.; Preut, H.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 559, p. 154 - 162
