(Z)-2-氯-2-(2-苯肼基)乙酸甲基合成路线 (共 14 条)
反应条件
triethylamine in benzene
20 h; Heating; Further byproducts given;
参考文献
Bruche, Luca; Zecchi,Gaetano
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1705 - 1706
反应条件
sodium azide; tri-n-butylhexadecylphosphonium bromide in water; benzene
T=40°C; 5 h;
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1427 - 1429
反应条件
1: 59 percent / sodium azide, hexadecyltributylphosphonium bromide / benzene; H2O / 5 h / 40 °C
2: 8 percent / benzene / 4 h / 80 °C
View Scheme
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1427 - 1429
反应条件
sodium ethanolate in diethyl ether
15 h; Ambient temperature;
参考文献
Bernard; Cocco; Maccioni; Plumitallo
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 4 p. 259 - 271