2-甲基-2,6,7,8-四氢-5H-苯并吡喃-5-酮合成路线 (共 6 条)
反应条件
in neat (no solvent)
T=20 - 120°C; 8 h; Microwave irradiationGreen chemistry;
参考文献
Edayadulla, Naushad; Lee, Yong Rok
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 10 p. 2963 - 2967
反应条件
4 A molecular sieve; titanium tetrachloride in dichloromethane
T=20°C; 24 h;
参考文献
Kurdyumov, Aleksey V.; Lin, Nan; Hsung, Richard P.; Gullickson, Glen C.; Cole, Kevin P.; Sydorenko, Nadiya; Swidorski, Jacob J.
Organic Letters, 2006 , vol. 8, # 2 p. 191 - 193
反应条件
(S)-3,3′-bis[3,5-bis(trifluoromethyl)phenyl]-1,1′-binaphthyl-2,2′-diyl hydrogenphosphate; sodium sulfate in toluene
T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Moreau, Julie; Hubert, Claudie; Batany, Jessika; Toupet, Loic; Roisnel, Thierry; Hurvois, Jean-Pierre; Renaudz, Jean-Luc
Journal of Organic Chemistry, 2009 , vol. 74, # 23 p. 8963 - 8973
反应条件
4 A molecular sieve; boron trifluoride diethyl etherate in dichloromethane
T=0°C; 48 h;
参考文献
Kurdyumov, Aleksey V.; Lin, Nan; Hsung, Richard P.; Gullickson, Glen C.; Cole, Kevin P.; Sydorenko, Nadiya; Swidorski, Jacob J.
Organic Letters, 2006 , vol. 8, # 2 p. 191 - 193
反应条件
4 A molecular sieve; boron trifluoride diethyl etherate in dichloromethane
T=0 - 20°C; 120 h;
参考文献
Kurdyumov, Aleksey V.; Lin, Nan; Hsung, Richard P.; Gullickson, Glen C.; Cole, Kevin P.; Sydorenko, Nadiya; Swidorski, Jacob J.
Organic Letters, 2006 , vol. 8, # 2 p. 191 - 193
反应条件
water
T=80°C; Domino Knoevenagel/6π-electrocyclization; 6 h;
参考文献
Jung, Ene Jin; Park, Byung Ho; Lee, Yong Rok
Green Chemistry, 2010 , vol. 12, # 11 p. 2003 - 2011