5,5-二甲基-2-苯基-1-吡咯啉-N-氧化物合成路线 (共 4 条)
反应条件
ammonium hydroxide; oxygen; copper diacetate
1.) Et2O, r.t., overnight, 2.) MeOH; Yield given. Multistep reaction;
参考文献
Janzen, Edward G.; Zhang, Yong-Kang; Haire, D. Lawrence
Magnetic Resonance in Chemistry, 1994 , vol. 32, # 12 p. 711 - 720
反应条件
ammonium hydroxide; air; copper diacetate
2.) MeOH; Multistep reaction;
参考文献
Janzen, Edward G.; Zhang, Yong-Kang
Journal of Magnetic Resonance, Series B, 1993 , vol. 101, # 1 p. 91 - 93
反应条件
nitric acid in acetonitrile
1 h; Heating; Title compound not separated from byproducts;
参考文献
Black, David St.C; Strauch, Richard J.
Australian Journal of Chemistry, 1988 , vol. 41, # 10 p. 1613 - 1619
反应条件
lithium aluminium tetrahydride in diethyl ether
T=0 - 5°C; 1.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Janzen, Edward G.; Zhang, Yong-Kang; Haire, D. Lawrence
Magnetic Resonance in Chemistry, 1994 , vol. 32, # 12 p. 711 - 720