5-氟-2,4-双(三甲硅氧)嘧啶合成路线 (共 4 条)
反应条件
ammonium hydroxide in tetrahydrofuran; methanol
参考文献
PCR, Inc.
Patent: US4024143 A1, 1977 ;
反应条件
pyridine; acetic anhydride; sodium hydrogencarbonate; benzaldehyde; tin(IV) chloride in methanol; chloroform; ethylene glycol
参考文献
Chugai Seiyaku Kabushiki Kaisha
Patent: US4415573 A1, 1983 ;
反应条件
ammonium sulfate
1 h; Heating;
参考文献
Ogilvie, Kelvin K.; Hamilton, Raymond G.; Gillen, Michael F.; Radatus, Bruno K.; Smith, Kendall O.; Galloway, Karen S.
Canadian Journal of Chemistry, 1984 , vol. 62, p. 16 - 21
参考文献
Piperno, Anna; Giofre, Salvatore V.; Iannazzo, Daniela; Romeo, Roberto; Romeo, Giovanni; Chiacchio, Ugo; Rescifina, Antonio; Piotrowska, Dorota G.
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 2798 - 2805