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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5814-81-3
合成路线
（共 9 条）
5814-81-3
→
反应条件
100-52-7
苯甲醛
+
123-11-5
大茴香醛
+
100-09-4
凯素灵
+
65-85-0
苯甲酸
反应条件
9,10-anthracenedicarbonitrile; oxygen in acetonitrile 6 h; Irradiationintermediate formation of 3-(4-methoxyphenyl)-5-phenyltrioxolane; Mechanism;
参考文献
Futamura, Shigeru; Kusunose, Shosaku; Ohta, Hiroyuki; Kamiya, Yoshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 1 p. 15 - 19
108-24-7
乙酸酐
+
5814-81-3
→
反应条件
反应条件
1: trans-(para-methoxy)stilbene oxide With Amberlyst 15; lithium bromide in acetonitrile T=-30°C; 2 h; 2: acetic anhydride With pyridine T=-30°C;
参考文献
Solladie-Cavallo, Arlette; Lupattelli, Paolo; Bonini, Carlo
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1605 - 1611
108-24-7
乙酸酐
+
5814-81-3
→
反应条件
24845-40-7
2-(4-甲氧基苯基)-1-苯基乙酮
反应条件
1: trans-(para-methoxy)stilbene oxide With Amberlyst 15; lithium bromide in acetonitrile T=-30°C; 2 h; 2: acetic anhydride With pyridine T=20°C;
参考文献
Solladie-Cavallo, Arlette; Lupattelli, Paolo; Bonini, Carlo
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1605 - 1611
5814-81-3
→
反应条件
24845-40-7
2-(4-甲氧基苯基)-1-苯基乙酮
反应条件
[ruthenium(2,2′-bipyridine)2Cl2]; carbon tetrabromide in acetonitrile T=20°C; 12 h; Irradiation;
参考文献
Guo, Lin; Yang, Chao; Zheng, Lewei; Xia, Wujiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 35 p. 5787 - 5792
5814-81-3
→
反应条件
5422-47-9
+
20498-67-3
对甲氧基-alpha-苯基苯乙醇
反应条件
palladium 10 on activated carbon; hydrogen; acetic acid in ethyl acetate T=20°C; P=760.051 Torr; 7 h; regioselective reaction;
参考文献
Blasio, Nadia Di; Lopardo, Maria Teresa; Lupattelli, Paolo
European Journal of Organic Chemistry, 2009 , # 6 p. 938 - 944
5814-81-3
→
反应条件
56913-16-7
反应条件
[ruthenium(2,2′-bipyridine)2Cl2]; carbon tetrabromide in acetonitrile 5 h; Irradiation; SolventReagent/catalyst; regioselective reaction;
参考文献
Guo, Lin; Yang, Chao; Zheng, Lewei; Xia, Wujiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 35 p. 5787 - 5792
5814-81-3
→
反应条件
5422-47-9
+
20498-67-3
对甲氧基-alpha-苯基苯乙醇
反应条件
palladium 10 on activated carbon; hydrogen; acetic acid in ethyl acetate T=20°C; P=760.051 Torr; 7 h; regioselective reaction;
参考文献
Blasio, Nadia Di; Lopardo, Maria Teresa; Lupattelli, Paolo
European Journal of Organic Chemistry, 2009 , # 6 p. 938 - 944
5814-81-3
→
反应条件
5422-47-9
反应条件
1: in ethyl acetate T=20°C; Inert atmosphere; 2: With formic acid; triethylamine in ethyl acetate T=0 - 20°C; Inert atmosphere; regioselective reaction;
参考文献
Kimachi, Tetsutaro; Nagata, Hiroyo; Kobayashi, Yusuke; Takahashi, Kaori; Torii, Eri; Ju-Ichi, Motoharu
Synlett, 2011 , # 3 art. no. U09710ST, p. 365 - 368
5814-81-3
→
反应条件
100-52-7
苯甲醛
+
123-11-5
大茴香醛
+
100-09-4
凯素灵
+
65-85-0
苯甲酸
反应条件
9,10-anthracenedicarbonitrile; oxygen in acetonitrile 6 h; Irradiationintermediate formation of 3-(4-methoxyphenyl)-5-phenyltrioxolane; Mechanism;
参考文献
Futamura, Shigeru; Kusunose, Shosaku; Ohta, Hiroyuki; Kamiya, Yoshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 1 p. 15 - 19
