4-烯丙氧基-3-氯苯甲醛合成路线 (共 4 条)
反应条件
1: 3-chloro-4-hydroxy-benzaldehyde With sodium hydride in tetrahydrofuran; DMF (N,N-dimethyl-formamide)
T=20°C; 1 h;
2: allyl bromide in tetrahydrofuran; DMF (N,N-dimethyl-formamide)
T=65°C; 18 h;
参考文献
ACTELION PHARMACEUTICALS LTD
Patent: WO2005/54215 A1, 2005 ;
Location in patent: Page/Page column 31-32 ;
反应条件
5,10,15,20-tetrakis-pentafluorophenyl-21H,23H-porphyrin iron(III) chloride; iodosylbenzene in dichloromethane
20 h; Ambient temperature;
参考文献
Komuro, Masakatsu; Nagatsu, Yoshio; Higuchi, Tsunehiko; Hirobe, Masaaki
Tetrahedron Letters, 1992 , vol. 33, # 34 p. 4949 - 4952
反应条件
1: N-chlorosuccinimide / CHCl3 / 72 h / Heating
2: 3.7 g / K2CO3 / acetone / 4 h / Heating
View Scheme
参考文献
Li, Dong Bo; Robinson, John A.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 7 p. 1233 - 1239
反应条件
potassium carbonate in acetone
4 h; Heating;
参考文献
Li, Dong Bo; Robinson, John A.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 7 p. 1233 - 1239