2,4,5-三甲基苯甲腈合成路线 （共 10 条）
反应条件
Pb(II) thiocyanate T=200 - 230°C;
参考文献
Rudenko; Salfetnikova; Vasil'ev
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 10 p. 1447 - 1470
反应条件
1: 85 percent / 37 percent HBr / acetic acid / 2 h / Ambient temperature 2: 43 percent / KOH, dihydrogen sulfide / H2O / 0.5 h / Heating 3: 27 percent / ethylnitrile, dicyclohexylcarbodiimide 4: 25 percent / CH2Cl2 / 16 h / Irradiation View Scheme
参考文献
Liebigs Annalen der Chemie, , # 6 p. 1025 - 1034
反应条件
1: 43 percent / KOH, dihydrogen sulfide / H2O / 0.5 h / Heating 2: 27 percent / ethylnitrile, dicyclohexylcarbodiimide 3: 25 percent / CH2Cl2 / 16 h / Irradiation View Scheme
参考文献
Liebigs Annalen der Chemie, , # 6 p. 1025 - 1034
反应条件
1: 27 percent / ethylnitrile, dicyclohexylcarbodiimide 2: 25 percent / CH2Cl2 / 16 h / Irradiation View Scheme
参考文献
Liebigs Annalen der Chemie, , # 6 p. 1025 - 1034
反应条件
in dichloromethane 16 h; Irradiation;
参考文献
Liebigs Annalen der Chemie, , # 6 p. 1025 - 1034
反应条件
pyridine; hydroxylamine hydrochloride 2 h; Heating;
参考文献
Tetrahedron, , vol. 47, # 3 p. 447 - 456
反应条件
Diazotization.durch Verseifen mit alkoh. Kali;
参考文献
Chemische Berichte, , vol. 18, p. 93
Justus Liebigs Annalen der Chemie, , vol. 237, p. 26
American Chemical Journal, , vol. 11, p. 7
反应条件
in benzene 16 h; Irradiationeffect of use of various solvents; Product distribution;
参考文献
Liebigs Annalen der Chemie, , # 6 p. 1025 - 1034
反应条件
tetrahydrofuran anschliessend mit wss.H2SO4;
参考文献
Hesse; Schroedel
Justus Liebigs Annalen der Chemie, 1957 , vol. 607, p. 24,30
反应条件
ethanol; sodium
substance of Kroemer;
参考文献
Kroemer
Chemische Berichte, 1891 , vol. 24, p. 2413
