N-己基-2-甲基-苯甲酰胺合成路线 (共 2 条)
反应条件
4-(N,N-dimethlyamino)pyridine; triphenylphosphine; 2aλ3-ioda-2,3-dioxa-cyclopenta[cd]indene-1,4-dione in chloroform
T=60°C; 8 h;
参考文献
Tian, Jun; Gao, Wen-Chao; Zhou, Dong-Mei; Zhang, Chi
Organic Letters, 2012 , vol. 14, # 12 p. 3020 - 3023
反应条件
1: With 4-(N,N-dimethlyamino)pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine in 1,4-dioxane
0.0333333 h; Inert atmosphere;
2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane
T=85°C; 15 h;
参考文献
Nordeman, Patrik; Odell, Luke R.; Larhed, Mats
Journal of Organic Chemistry, 2012 , vol. 77, # 24 p. 11393 - 11398