1-苯基-1,4-戊二酮合成路线 （共 177 条）
反应条件
1: aq. KOH
View Scheme
参考文献
Farnum,D.G. et al.
Journal of Organic Chemistry, 1971 , vol. 36, # 5 p. 698 - 702
反应条件
hexaphenyldistannathiane, bis(triphenyltin)sulfide; boron trichloride in toluene
2 h; Heating;
参考文献
Freeman, Fillmore; Kim, Darrick S. H. L.; Rodriguez, Eloy
Journal of Organic Chemistry, 1992 , vol. 57, # 6 p. 1722 - 1727
反应条件
2: ethanolic NaOH-solution
View Scheme
参考文献
Buu-Hoi et al.
Journal of Medicinal and Pharmaceutical Chemistry, 1959 , vol. 1, p. 23,26
反应条件
hydrogen; palladium on activated charcoal in methanol
T=20°C; 24 h;
参考文献
Suzuki, Hideyuki; Nishioka, Hiromi; Takeuchi, Yasuo
Tetrahedron Letters, 2012 , vol. 53, # 28 p. 3686 - 3688
反应条件
ammonium hydroxide; titanium(III) chloride in methanol
T=20 - 25°C; pH=10 - 11; 0.0833333 h;
参考文献
Clerici, Angelo; Pastori, Nadia; Porta, Ombretta
European Journal of Organic Chemistry, 2002 , # 19 p. 3326 - 3335
反应条件
indium; acetic acid in toluene
24 h; Inert atmosphereReflux;
参考文献
Lee, Hyunseung; Kim, Byeong Hyo
Tetrahedron, 2013 , vol. 69, # 32 p. 6698 - 6708
反应条件
iodine in tetrahydrofuran
T=20°C; 7 h;
参考文献
De, Surya K.
Heteroatom Chemistry, 2008 , vol. 19, # 6 p. 592 - 595
反应条件
indium; acetic acid in toluene
1.5 h; Inert atmosphereReflux; TemperatureConcentrationTime;
参考文献
Lee, Hyunseung; Kim, Byeong Hyo
Tetrahedron, 2013 , vol. 69, # 32 p. 6698 - 6708
反应条件
sodium hydroxide in water
4 h; Reflux;
参考文献
Peloquin, Andrew J.; Stone, Rebecca L.; Avila, Sarah E.; Rudico, Erlyn R.; Horn, Christopher B.; Gardner, Kim A.; Ball, David W.; Johnson, Jane E. B.; Iacono, Scott T.; Balaich, Gary J.
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 6371 - 6376
参考文献
Paal
Chemische Berichte, 1884 , vol. 17, p. 916,2757
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Borsche; Fels
Chemische Berichte, 1906 , vol. 39, p. 1928
