1-苯基-1,4-戊二酮合成路线 (共 177 条)
反应条件
copper(II) oxide; copper dichloride in water; acetone
参考文献
Journal of the American Chemical Society, , vol. 94, # 24 p. 8641 - 8642
反应条件
hydrogenchloride in acetic acid T=80°C; 0.333333 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 5 p. 1371 - 1378
反应条件
tetrabutylammonium hexanitratocerate(IV); potassium carbonate in acetonitrile T=0°C; 2 h;
参考文献
Kohno, Yasushi; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 1 p. 322 - 329
反应条件
ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride; acetic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene 24 h; Inert atmosphereReflux;
参考文献
Pridmore, Simon J.; Slatford, Paul A.; Taylor, James E.; Whittlesey, Michael K.; Williams, Jonathan M.J.
Tetrahedron, 2009 , vol. 65, # 44 p. 8981 - 8986
反应条件
1: 1.) butyl-lithium, 2.) copper(I) iodide 2: MCPBA / diethyl ether / 0 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1695 - 1706
反应条件
sodium carbonate in methanol; water 6 h; Heating;
参考文献
Mackay, Donald; Dao, Le H.; Dust, Julian M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2408 - 2416
反应条件
(acetylmethylene)triphenylphosphorane in dichloromethane T=25°C;
参考文献
Chemical Communications, , # 3 p. 333 - 334
反应条件
potassium cyanide in N,N-dimethyl-formamide 0.5 h; Ambient temperature;
参考文献
Miyashita, Akira; Suzuki, Yumiko; Okumura, Yoko; Iwamoto, Ken-Ichi; Higashino, Takeo
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 1 p. 6 - 11
反应条件
ZnCl2*Et3N*t-BuOH in benzene T=20°C; Condensation; 72 h;
参考文献
Nevar; Kel'in; Kulinkovich
Synthesis, 2000 , # 9 p. 1259 - 1262
反应条件
indium monobromide in tetrahydrofuran T=20°C; 24 h;
参考文献
Synlett, , # 7 p. 1187 - 1190