反应条件
in dichloromethane; water
byproducts: ((CH3O)3C6H2NC)2C10H6; (N2); using Schlenk techniques; dissolving in CH2Cl2; shaking with satd.K2C2O4 aq. soln. for 10 min; sepn. of org. phase; washing with H2O; drying with Na2SO4, evapn. in vac., chromy. on silica using 10;0.5 hexane/triethylamine as eluent;
参考文献
Scarel, Alessandro; Axet, M. Rosa; Amoroso, Francesco; Ragaini, Fabio; Elsevier, Cornelis J.; Holuigue, Alexandre; Carfagna, Carla; Mosca, Luca; Milani, Barbara
Organometallics, 2008 , vol. 27, # 7 p. 1486 - 1494
