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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1,2-二溴苯
合成路线
（共 406 条）
766-09-6
N-乙基哌啶
+
583-53-9
1,2-二溴苯
→
反应条件
108-86-1
溴代苯
+
4096-20-2
N-苯基哌啶
+
54509-73-8
+
71-43-2
反应条件
tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide T=40°C; electroreduction: Pt electrode vs. Ag/Ag+;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 7 p. 2671 - 2673
71-43-2
+
583-53-9
1,2-二溴苯
→
反应条件
108-86-1
溴代苯
+
92-52-4
+
2052-07-5
反应条件
T=25°C; 20 h; Irradiation;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 10 p. 3122 - 3126
583-53-9
1,2-二溴苯
→
反应条件
19467-24-4
+
22069-99-4
反应条件
1: With tert.-butyl lithium in tetrahydrofuran; diethyl ether; pentane T=-120°C; 0.5 h; 2: With diclazuril in tetrahydrofuran; diethyl ether; pentane T=-120 - -110°C; 0.5 h; Further stages.;
参考文献
Bettinger, Holger F.; Filthaus, Matthias
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9750 - 9752
457644-50-7
+
583-53-9
1,2-二溴苯
→
反应条件
19227-07-7
+
275-51-4
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
708-06-5
+
583-53-9
1,2-二溴苯
→
反应条件
1931-53-9
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in N,N-dimethyl-formamide T=130°C; 12 h; Inert atmosphere;
参考文献
Wang, Sizhuo; Xie, Kai; Tan, Ze; An, Xiangyu; Zhou, Xingjian; Guo, Can-Cheng; Peng, Zhihong
Chemical Communications, 2009 , # 42 p. 6469 - 6471
90-15-3
+
583-53-9
1,2-二溴苯
→
反应条件
200-23-7
反应条件
caesium carbonate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide T=140°C; Cyclization; 24 h;
参考文献
Terao, Yoshito; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 10 p. 2345 - 2350
673-22-3
+
583-53-9
1,2-二溴苯
→
反应条件
3722-52-9
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in N,N-dimethyl-formamide T=130°C; 12 h; Inert atmosphere;
参考文献
Wang, Sizhuo; Xie, Kai; Tan, Ze; An, Xiangyu; Zhou, Xingjian; Guo, Can-Cheng; Peng, Zhihong
Chemical Communications, 2009 , # 42 p. 6469 - 6471
105-36-2
+
100-47-0
+
583-53-9
1,2-二溴苯
→
反应条件
36779-16-5
反应条件
1: ethyl bromoacetate; benzonitrile With methanesulfonic acid; zinc in tetrahydrofuran Blaise reaction; RefluxInert atmosphere; 2: ortho-dibromobenzene With copper(l) iodide; 1,10-phenanthroline; potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Kim, Ju Hyun; Lee, Sang-Gi
Synthesis, 2012 , vol. 44, # 10 p. 1464 - 1476
→
反应条件
1076-69-3
反应条件
tetrabutyl ammonium fluoride; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=101°C; Stille reaction; 15 h;
参考文献
Herve, Agnes; Rodriguez, Alain L.; Fouquet, Eric
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1953 - 1956
629-03-8
+
583-53-9
1,2-二溴苯
→
反应条件
1076-69-3
反应条件
1: 1,6-dibromo-n-hexane With Sn[N(SiMe3)2]2 in tetrahydrofuran T=20°C; 20 h; 2: ortho-dibromobenzene With tetrabutyl ammonium fluoride; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=101°C; Stille reaction; 15 h;
参考文献
Herve, Agnes; Rodriguez, Alain L.; Fouquet, Eric
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1953 - 1956
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