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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1,2-二溴苯
合成路线
（共 406 条）
1747-60-0
2-氨基-6-甲氧基苯并噻唑
+
583-53-9
1,2-二溴苯
→
反应条件
1771-19-3
3-甲氧基-10H-吩噻嗪
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in dimethyl sulfoxide T=170°C; 34 h; Inert atmosphere;
参考文献
Beresneva; Abele
Chemistry of Heterocyclic Compounds, 2012 , vol. 48, # 9 p. 1420 - 1422
Khim. Geterotsikl. Soedin., 2012 , vol. 48, # 9 p. 1521 - 1524,3
536-74-3
苯乙炔
+
583-53-9
1,2-二溴苯
→
反应条件
1207-95-0
反应条件
1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 20 °C / |Inert atmosphere 2: potassium ethylxanthate; copper diacetate; (R)-(+)-1,1'-binaphthyl-2,2'-diamine / N,N-dimethyl-formamide / 48 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Prasad; Sekar
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1659 - 1665
27607-77-8
三氟甲磺酸三甲基硅酯
+
583-53-9
1,2-二溴苯
→
反应条件
反应条件
1: ortho-dibromobenzene With tert.-butyl lithium in tetrahydrofuran; diethyl ether; pentane T=-120 - 20°C; 0.666667 h; 2: trimethylsilyl trifluoromethanesulfonate in tetrahydrofuran; diethyl ether; pentane T=-120 - -110°C; 0.5 h; Further stages. Further byproducts.;
参考文献
Bettinger, Holger F.; Filthaus, Matthias
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9750 - 9752
13922-41-3
1-萘硼酸
+
583-53-9
1,2-二溴苯
→
反应条件
18937-92-3
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in toluene T=85°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Liu, Feng; Xie, Ling-Hai; Tang, Chao; Liang, Jing; Chen, Qing-Quan; Peng, Bo; Wei, Wei; Cao, Yong; Huang, Wei
Organic Letters, 2009 , vol. 11, # 17 p. 3850 - 3853
583-53-9
1,2-二溴苯
→
反应条件
18937-92-3
反应条件
1: triisopropyl borate; n-butyllithium / toluene; tetrahydrofuran; hexane / 2.08 h / -70 - 20 °C 2: aq. HCl / toluene; tetrahydrofuran; hexane / 0.5 h / 20 °C 3: 31.38 g / toluene / 2 h / Heating 4: 70 percent / aliquate 336; Na2CO3 / tetrakis(triphenylphosphine)palladium(0) / toluene; H2O / 5 h / 90 °C View Scheme
参考文献
Wang, Tein-Fu; Lin, Ching-Lung; Chen, Chih-Neng; Wang, Tan-Ching
Journal of the Chinese Chemical Society, 2007 , vol. 54, # 3 p. 811 - 816
104-86-9
对氯苄胺
+
13939-06-5
六羰基钼
+
583-53-9
1,2-二溴苯
→
反应条件
131523-32-5
反应条件
palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; di-(1-adamantyl)-n-butylphosphine in toluene T=100°C; 16 h; Sealed tubeInert atmosphere;
参考文献
Wu, Xiao-Feng; Oschatz, Stefan; Sharif, Muhammad; Flader, Anika; Krey, Lisa; Beller, Matthias; Langer, Peter
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3581 - 3585
451-40-1
二苯基乙酮
+
583-53-9
1,2-二溴苯
→
反应条件
13054-95-0
反应条件
caesium carbonate; triphenylphosphine; palladium diacetate in o-xylene 8 h; RefluxInert atmosphere;
参考文献
Idemitsu Kosan Co., Ltd.; Sony Corporation
Patent: EP2163550 A1, 2010 ;
Location in patent: Page/Page column 47-48 ;
451-40-1
二苯基乙酮
+
583-53-9
1,2-二溴苯
→
反应条件
13054-95-0
反应条件
caesium carbonate; triphenylphosphine; palladium diacetate in o-xylene Cyclization; 2 h; Heating;
参考文献
Terao, Yoshito; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 10 p. 2345 - 2350
85199-06-0
2,5-二甲基苯硼酸
+
583-53-9
1,2-二溴苯
→
反应条件
2523-39-9
3-甲基-9H-芴
反应条件
palladium diacetate; potassium carbonate; tri-cyclo-hexyl-phosphine; 2,2,2-trimethylacetic acid in N,N-dimethyl acetamide T=140 - 150°C; 5 h;
参考文献
Liu, Tao-Ping; Xing, Chun-Hui; Hu, Qiao-Sheng
Angewandte Chemie - International Edition, 2010 , vol. 49, # 16 p. 2909 - 2912
39536-36-2
+
583-53-9
1,2-二溴苯
→
反应条件
2622-73-3
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene T=140°C; 24 h; Molecular sieveInert atmosphere; regiospecific reaction;
参考文献
Zhao, Dongbing; Hu, Junyi; Wu, Ningjie; Huang, Xiaolei; Qin, Xurong; Lan, Jingbo; You, Jingsong
Organic Letters, 2011 , vol. 13, # 24 p. 6516 - 6519
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