反应条件
1: triisopropyl borate; n-butyllithium / toluene; tetrahydrofuran; hexane / 2.08 h / -70 - 20 °C
2: aq. HCl / toluene; tetrahydrofuran; hexane / 0.5 h / 20 °C
3: 31.38 g / toluene / 2 h / Heating
4: 40 percent / aliquate 336; Na2CO3 / tetrakis(triphenylphosphine)palladium(0) / toluene; H2O / 5 h / 90 °C
View Scheme
参考文献
Zhou, Jun; Yang, Weijun; Wang, Binjie; Ren, Hongjun
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12293 - 12297
Angew. Chem., 2012 , vol. 124, # 49 p. 12459 - 12463,5